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rJ41 Jul zurio 14;1l. ZV140UJ4`1 ririn rLUUM t-Hua ❑u <br /> MINIMUM VERIFICATION LABORATORY ANYAL)'SI5 <br /> } ee', <br /> TAM< cat <br /> QxYGEVArF$ <br /> caes <br /> nrAiS <br /> TANK TPtI{'i TFH-A BTX&E CL HC TOTAL MTBEICA.P/ FC$ <br /> ti C0NTENT 9 8015 $015 8020 $010 LEAD 8020 �6 DL'E $270 <br /> >;:BE. A",, 8080 <br /> $260 8260 8260 8240 7420 $260 . TAME)) ,gyp <br /> yds. 8260 7421 8:E0 <br /> LE�.DEDGAS X X X X <br /> UNL GAS X X X <br /> DIESEL X X <br /> V-� <br /> KEROSE:LtiE X X X <br /> UNTK FUEL X X X X X <br /> PROD,OIL X X X <br /> CHLOR. <br /> SOI.4'EIvAS X X X C <br /> NONCFLOR X <br /> SOI,VEvAS X X <br /> WAS=)- <br /> (istD OIL X X X X 3, <br /> Ali analysis mcdauds are the designated EPA methods described in EPA SW 846,Third Edidon. i hose methods nat found in S'N' <br /> $a6 a ,spe l:caliy nosed below. Refer to the'"SWRCB LITFT Field Manual",Appendix D(B),Table 3-5 on pate A M for <br /> minim4m detection limits for motor vehicle fuel(gasoline and diesel)- Refer to"Tri-Regional Board Staff Arnott menQ4ems for <br /> iai Evaluation and Inves igati6a of UST's"for the waste and motor oil minimum detection limits. <br /> Detect-an Limits that remain below the MCL,STLC or Allowable Limit of the Contaminant in questl.ost will be accepted, <br /> horeever labaratw-y shall utilize the most conservative method- <br /> LABORATOR i:1NAI YSES TFRi�MOL00Y: <br /> TRR-G Total Pctmlcum Hydrocarbon,Gasoline,GClFM(5030)8015 mod or GC/MS$260 <br /> TPH-D Total petroleum Hydrocarbon,Diesel,GC/PID(3550),8015 mod or GC/ML9 8260 <br /> BTX&E Benzene,Toluene.Xylene&Ethyl Benzene,GVFM 8020 or GC/MS 8260 <br /> CL HC ChlonnrW Hydrocarbon,GC/HSD 8010,GCIMS 8240 or 8260 . <br /> TOTAL LEAD Total lead,AA 7420, AA 7421 or ICP-AES 6010 <br /> OX fGENATES D1TBE,ETRE,TAME,DIPS,&TBA GC/MS 8260(For MTBE screen only you may use 8020) <br /> METALS ICAP w AA Induetivcly Coupled plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spw=uicty 7000. <br /> Metals;Cadmium,Chromium III and VI,Lead,Zinc and nickel. <br /> PC- . Folychiminated 9iphenyls,GUMS 8270 or 8080 <br /> GC-FID C-as Chromatography.Flamc Ionization Dctcct.ion <br /> McP.,'=.ad 303E Acid digestion <br /> Method 5540 Soxhiet sample prcparation <br /> Method 3530 Sonication sample preparation,extraction method <br /> Maihcd 3030 Pares and trap sample preparation <br /> Quality Assurance/QualkyControl <br /> *totes: To avoid false positive detection of benzene,benzene-free solvents are to be used. Fused capillary columns aro preferwi,to pacced - <br /> col'utnrs;a packed coicem nay be used as a"first cut"with"dirty"samples or once the hydrocarbons have beta chw acterized and proper QAfQC .. .,� <br /> is followed. <br /> For drink:n,+rac-.r snar✓s EPA recommends that the 500 series for volatile organic should be used in preference to Esse 600 scnes because the <br /> d-L^.cd011 limit,we[oxer and tic QA/QC is better. $=pies exhibiting any Icvel of heavy rectal mmamination may aeGtdra furet!cr aneysis.EID <br /> t'ecommeads holcmg those sdrples until disposal is indicated- <br /> E42:00146 <br /> ndicated.EH?i436 (Revi2eciI0116/03) Page 8 <br />