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3D <br /> SOIL SEMIVOSILE MATRIX SPIKE/MATRIX SPIKE DUOATE RECOVERY <br /> Lab Name: PAN-AG ENVIRO LABS Contract: <br /> Project No.: Site: Location: Group: <br /> Matrix Spike - Sample No.: 86-9408-274 Level: (low/med) LOW <br /> SPIKE SAMPLE MS MS QC. <br /> ADDED CONCENTRATION CONCENTRATION % LIMITS <br /> COMPOUND (ug/Kg) (ug/Kg) (ug/Kg) REC # REC. <br /> Phenol 6700 0 3400 51 * (52-180) <br /> Chlorophenol 6700 0 3600 54 (50-204) <br /> 1,4-Dichlorobenzene 3300 0 2200 67 (28-104) <br /> N-Nitroso-di-n-propylamine 3300 0 2600 79 (41.126) <br /> 1,2,4-Trichlorobenzene 3300 0 2400 73 38-107) <br /> Chloro-3-methylphenol 6700 0 3900 58 (52-206) <br /> Acenaphthene 3300 0 2400 73 (31-137) <br /> Nitrophenol 6700 0 4800 72 (22-114) <br /> ,4-Dinitrotoluene 3300 0 2400 73 (28-89) <br /> entachlorophenol 6700 0 3500 52 (34-218) <br /> Pyrene 3300 0 1 2900 88 (31-142) <br /> SPIKE MSD MSD <br /> ADDED CONCENTRATION % % QC LIMITS <br /> COMPOUND (ug/Kg) (ug/Kg) REC # RPD # RPD REC. <br /> Phenol 6700 3400 51 * 0 35 (52-180) <br /> -Chlorophenol 6700 3600 54 0 50 (50-204) <br /> 1,4-Dichlorobenzene 3300 2100 64 5 27 (28-104) <br /> N-Nitroso-di-n-propylamine 3300 2500 76 4 38 (41-126) <br /> 1,2,4-Trichlorobenzene 3300 2400 73 0 23 (38-107) <br /> -Chloro-3-methylphenol 6700 3900 58 0 33 52-206) <br /> Acenaphthene 3300 2400 73 0 19 (31-137) <br /> -Nitrophenol 6700 4800 72 0 50 22-114) <br /> ,4-Dinitrotoluene 3300 2400 73 0 47 (28-89) <br /> Pentachlorophenol 6700 3700 1 55 6 47 34-218) <br /> Pyrene 3300 2800 85 4 36 (31-142) <br /> # Column to be used to flag recovery and RPD values with an asterisk <br /> * Values outside of QC limits <br /> RPD: 0 out of 11 outside limits <br /> Spike Recovery: 2 out of 22 outside limits <br /> Comments: <br /> FORM III SV-2 3/90 <br /> 33 <br />