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PIMUM VERIFICATION LABORATORY <br /> NALYSIS <br /> 'PANIC TANK TPH-G TPH-D BTX & E CL HC TOTAL, EDB METALS P <br /> # CONTENTS 8015 8015 80217 8010 LEAD CB <br /> 8260 8260 8250 ICAP/ 8270 <br /> ' 824t7 7420 82240 AFS or 8080 <br /> 7421 AA <br /> LEADED <br /> GAS X X <br /> X X <br /> UNL GAS X X <br /> DIESEL X X <br /> KEROSENE X X <br /> UNK FUEL X X X X X <br /> ' PROD. OIL X X <br /> CHLOR. <br /> ' SOLVENTS X X <br /> NONCHLOR <br /> SOLVENTS X X X <br /> WASTEI <br /> USED OIL X X X X X X <br /> All analyses methods are designated EPA methods described in EPA SW <br /> 84x5, Third Edition. `Those methods not found <br /> in SW 846, are specifically noted below. Refer to the -SWRCB LUFT Field ManuaI", Appendix A-20, Table 3-5 for <br /> t detection limits of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff Recommendations for <br /> Initial Evaluation and Investigation of UST's" for the waste and motor oil detection limits. <br /> Detection Limits that remain below the NICs, STLC or Allowable Limit of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPH`G Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 8015 mod or GC/MS 8260 <br /> ' TPH-D Total Petroleum Hydrocarbon, Diesel, GC/FTD (3550), 8015 mod or GGMS $26p <br /> BTX & E Benzene, Toluene, Xylene& Ethyl Benzene, GC/PID 8020 or GC/MS 8260 <br /> CL HC Chlorinated Hydrocarbon, GC/1-ISD 8010, GC/MS 8240 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES 5010 <br /> EDB Ethylene dibromide (DHS-AB 1803 G <br /> GC-FID Gas Ch ), GMS 8240 (DHS-LUPI) <br /> Chromatography, Flame Ionization Detection <br /> ' ICAP or AA Inductively Coupled plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> FCB Spectrometry 7000. Metals: Cadmium, Chromium III and Vi, Lead, Zinc and Nickel. <br /> PoIychIorinated Biphenyls, GC/MS 8270 or 8080 <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> ' Notes: To avoid false Positive detei <br /> on of benzene, benzene-free solvents are to be used. Fused capillary columns are <br /> preferred to packed columns; a packed column may be used as a 'first cut" witli "dirty" samples or once the hydrocarbons <br /> have been characterized and proper QA/AC is followed. <br /> For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600 <br /> series because the detection Iimits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal <br /> contamination may require further analysis. PHS-EHD recommends ]folding these samples until disposal is indicated. <br /> EH 23 048 (Revised 7/I0/92) Page 8 <br />