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GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr. Turlock.CA 95380 Phone(209)669-0100 Fm(209)593-2212 <br /> email: info®gtoanalyticallab.eom <br /> Report# 135130302 Project: 4445 N. Pershing,Stockton,Ca.95204 Date: 04/15/15 <br /> Jim Thorpe, Inc. Date Recd: 04/03/15 <br /> P.O Box 357 <br /> Lodi,CA 95241 <br /> Volatile Organic Chemistry- Quality Control <br /> GeoAnalytical Laboratories, Inc. <br /> Reporting Spike Source %REC RPD <br /> Anal to Result Limit Units Level Result % EC Limits RPD Limit Notes <br /> Batch 8001049-EPA 5030 Prepared&Analyzed:04/14/15 <br /> Blank(8001049-BLKI) <br /> 1,2-Dichlormthane ND 5.0 ug/kg <br /> Di-isopropyl Ether(DIPE) ND 10.0 " <br /> Ethanol ND 400 " <br /> Ethyl ten-Butyl Ether(E'rBE) ND 10.0 " <br /> Ethylene dibromide ND 10.0 " <br /> Methyl ten-Butyl Ether(MTBE) ND 10.0 " <br /> Ten-Amyl Methyl Ether(TAME) ND 10.0 " <br /> ten-Butanol(TBA) ND 200 <br /> Gasoline ND 1.0 mg/kg <br /> Surrogate:/,2-Dichloror/hane-d4 0.0222 0.02000 /11 71-132 <br /> Surrogate:2-Bromo-/-Chloropropane 0.0107 •• 0.02000 /04 71-134 <br /> Surrogate'4-Bromo/luoroben_ene 0.0177 0.01000 88 74-131 <br /> LCS(8001049-BSI) _ <br /> I.-Dichlormthane 65.8 5.0 ug/kg 60.00 110 80-120 <br /> Di-isopropyl Ether(DIPE) 60.4 10.0 60.00 101 80-120 <br /> Methyl ten-Butyl Ether(MTBE) 62.7 10.0 60.00 104 80-120 <br /> "fen-Amyl Methyl Ether("FAME) 57.7 10.0 60.00 96 80-120 <br /> Gasoline 1.6 1.0 mg/kg 1.500 103 80-120 <br /> Surrogate: 1,2-Dichlaroe1hane-d4 0.0201 0.02000 100 72-132 <br /> Surrogate:2-Bron, -IChloropropane 0.0205 0.02000 103 7/-134 <br /> Surrogate:4-Bromofluorobencene 0.0188 0.02000 94 74-132 <br /> Matrix Spike(B001049-MSI) Source: B5D0302-01 _ <br /> 1;2-Dichlormthane 61.6 5.0 ug/kg 60.00 ND 103 69-140 <br /> Di-isopropyl Ether(DIPE) 57.3 10.0 60.00 ND 95 68.134 <br /> Mcthyl ten-Butyl Ether(MTBE) 58.3 10.0 60.00 ND 97 76-179 <br /> "ren-Amyl Methyl Ether(TAME) 54.5 10.0 60.00 ND 91 69.140 <br /> Gasoline 1.7 I.0 mg/kg 1.500 ND 113 63.143 <br /> Sirrogare: 1,1-Dichlorcethane-d4 0.0194 0.02000 97 72-132 <br /> Snrrogare:2-Bromo-/-('hloropropane0.0184 0.01000 91 7/-/34 <br /> Surrogate:4-Brom0fluorobencenr0.0185 0.01000 93 74-/31 <br /> Certification#2585 <br />