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EXCELCHEM <br /> ENVIRONMENTAL LABS <br /> 500 Giuseppe Court, Suite 9 <br /> Roseville, CA 95678 <br /> Phone#: (916) 773-3664 Fax#: (916) 773-4784 <br /> ANALYSIS REPORT <br /> Attention: Mr. Patrick Fischer Date Sampled: 10-24-96 <br /> ESPANA GEOTECHNICAL Date Received: 10-29-96 <br /> 502 Giuseppe Court, Suite 11 Date Analyzed: 11-05-96 <br /> Roseville, CA 95678 <br /> Project : E168-1/Lodi Rail/Multimodal Station Matrix: Soil <br /> Sample ID: 11-2 <br /> Lab 11): 51096507 <br /> Reporting Measured <br /> Compound Limit(ppb) Value(ppb) <br /> Dichlorodifluoromethane 10 ND <br /> Chloromethane 10 N D <br /> Vinyl Chloride 10 ND <br /> Bromomethane 10 ND <br /> Chloroethane 10 ND <br /> Triclmlorofluorometlmane 10 ND <br /> 1,1-Dichloroethene 10 ND <br /> Methylene Chloride 10 ND <br /> Trans-l,2-Dichloroethene 10 ND <br /> 1,1-Dichloroethane 10 ND <br /> Chloroform 10 ND <br /> 1,2-Dichloroethane 10 ND <br /> Dibromochloromethane 10 ND <br /> 1,1,1-Trichloroethanc 10 ND <br /> Carbon Tetrachloride 10 ND <br /> Trichloroethene 10 ND <br /> 1,2-Dichloropropane 10 ND <br /> Bromodichloroniethane 10 ND <br /> Cis-1,3 Dichloropropene 10 ND <br /> Trans-1,3 Dichloropropene 10 ND <br /> 1,1,2-Trichloroethane 10 ND <br /> Tetrachloroethene 10 ND <br /> Chlorobenzene 10 ND <br /> Bromoform 10 ND <br /> 1,1,2,2-Tetrachlorobenzene 10 ND <br /> 1,3-Dichlorobenzene 10 ND <br /> 1,4-Dichlorobenzene 10 ND <br /> 1,2-Dichlorobenzene 10 ND <br /> ppb=parts per billion=ngig=nanograms per gain <br /> 1,411 =Not detected Compound(s)may be present at concentrations below the reporting limit. <br /> Surrogate Recoveries - 1,2-Dichloroethaned-4 99% <br /> Toluene-d8 100% <br /> 4-Bromofluorobenzene 95% <br /> ANALYTICAL PROCEDURES <br /> HV--Halogenated Volatiles are measured first by extraction(EPA method 5030)then by using EPA Method 8240 which utilizes a purge and trap <br /> interfaced to a gas chromatograph(GC)equipped with a mass spectrometer. <br /> I1-11-96 <br /> ab ratory Representative Date Reported <br /> £XCELCHEM EN;JRONMEATAL LABS IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SEM ICES AS A HA.ZARDOI:S WASTE TESTING LABORATORY <br /> (Cati6cetion No.t 760) <br />