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111'07/2032 J 1'32 2094#3 F1FTH FLULF F'G;raL OF. <br /> • <br /> MINIMUM VI=RIFICATION LA84RATORY ANALYSIS <br /> TANK TANK TPH-GOXYGEN <br /> TPH-17 B7X R E CL,1IC TOTAI. MTEE ATES ]WETS, F'GB <br /> CC]NTEN1"S 8CI15 11015 8020 8410 LEAD 8020 (MT6E. <br /> , <br /> 8260 8260 8260 8240 7420 8260 T9A,1�[PE1CAP/ B27G <br /> 8260 7421 $TSL. ABS or 5050 <br /> TAJAE) p A <br /> 52GD <br /> LEADED GAS x x X <br /> L',NL GAS ,C X <br /> DIESEL X X <br /> kE'ROSENTE 'X I X X <br /> i <br /> L>R'K FUEL x X I X X 3£ <br /> PROD.OIL X I X X <br /> CHLOR. <br /> SOLVENTS I X X X <br /> NONCHLOR <br /> SOLVENTS X X <br /> WASTE= <br /> USED OTL X X X X 30 X <br /> Al analysis method:arc the designated EPA methoiis disc 31n aA SW 946 <br /> xd i ,Third EditioaT Those methods not found in SW 846 arc <br /> specifically rioted below_ Rcfer to rhe"SWRCB .L[JFT Field Manual",Appendix D (z3),Table 3-5 on page A20 for= nitro,rn detection <br /> limits for rrlotor vehicle fuel (gasoline and diesel). Refer To "Tri-I24ona1 Board Staff Recotnmendations for Initial Evaluation anc <br /> Investigation of USTs" for, the waste and motor oil minimntn detection Betties. Detection limits that rerrntin below the MCL,STLC bs <br /> Allowable Limit of the contamin9nt in question will I je lecelpted,however laboratory shsW Utilize the most conservative method. <br /> I <br /> LABORATORY ANALYSES TERN[11�+rJLOGY: <br /> ?FI t-O Total Petroleum T3ydrocarhon,Gasoline,GC1FID(5630)8015 rood or GC1MS 926() <br /> TPH-D Total Petroleum i tydrotarbon,Diesel,GC-TD(35501 6015 mod or GCIMS 8260 <br /> BTX&£Benzene,Toluene,Xylcnc&Ethyl Benzeat,GCRM 8024 or GC,IMS B260 <br /> CL HC Chlorinated Hydrocarbon,GCIHSD 8010.GC/MS$-740 or 82601 <br /> TOTAL LEAD 'Total lead,AA 7420, AA 7421 or ICP-AES 6010 <br /> OXYGENATEZ MTBE,ETRE,TA-N1E,DIPS,&TBA O&MS 8260(For hitm Sacco only you mayusc 8024) <br /> METALS ICRP or AA Inductively Couplcd Plasma Atomic Emission Speetromecry oo10 or Atomic Absorption Speetromerry 7704. Metals: <br /> CAdmium.Chm"tim III end VI,Lead,7Anc Anti Nickel, <br /> PCO Polychlorinated Biphenyls,G&MS 8270 or 8D80 <br /> CC-FID Gas Chronatography,flame Ionization Detection <br /> Mcthod 3050 Acid digestion <br /> Method 3540 Soxhlet sample pre ration <br /> Method 3550 Sonication sample prima ation,extraction thod <br /> Method 5030 Purgc and trap sanT,pie preparation <br /> Q-A/QC Qrualivy Assurance/Quality Control <br /> Note,; To avoid false positive detection of ben2.enc,benzene-free solvents sre to be used, Fused capillary columns am preferred to p=Pcd solumuns;a <br /> packed colunm may be used as a"first tut"with."dirty"samples or once the hydroc4rbon5 have been chararttrizcd and proper QAIQC is°ojlau+ed_ For <br /> drinking water e011TCC6,EPA recommends that the 500 series for volatile organic should be used in preference t0 the 600 series because the dot-action <br /> limits are lower and the QA/QC is btacr. Sarnplcs cxhiblting any level of hca4y metal W ntamination tray squire farther winlysis.PUS-Ell!) <br /> recoturatuds holding those samples until disposal is indicated, <br /> EH 23 046 (Revised 05/04'00) p <br />