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SAN a027 LQUIk4 L©C'AL HE2�FIPH DI ST'Ft2 �T <br />Total Petroleum Hydrocarbon, Gasoline <br />TANK CLOSURE PLAN REVIEW CHECKLIST - MINIMUM VERIFICATION LAB ANALYSES <br />Total Petroleum Hydrocarbon, Diesel <br />NK TANK CONTENTS <br /># Waste Product <br />TPH-G TPH--D TEPH BTX&E CL HC TEL I EDB METALS <br />GC -FID GC -FID (3550) (8020) (8010) (DOHS) <br />PCB <br />(ICP- <br />(5030) (5030) (3540) (8240) AES) <br />rr-7 <br />(8270) <br />(8080) <br />LEADED GASOLINE <br />.____ ...___....._....__,......._.......__..._.................. ... <br />... _._ _._................. .._..._......._.. _ <br />Gas Chromatography Flame Ionization Detector <br />Inductively Coupled Plasma Atomic Emission Spectrometry or Atomic <br />UNL GASOLINE <br />Method <br />Method 3540 <br />QA/QCQuality <br />..._._.....,_._ <br />DIESEL <br />_---._---- _....._.__.__.__. ........ <br />proper QA/QC is followed. <br />KEROSENE <br />.... <br />for larellower <br />nce tostheP600esermesdbecausetthe5detection <br />. <br />UNKNOWN FUEL <br />liimitsies <br />and <br />_...._...._..._....__...__.._..._.._.._ <br />OIL <br />.................. _...._.._...._. ....._........ <br />............................_.__................._......._.__.........._._._.__................_. <br />CHLOR. SOLVENTS <br />..................... <br />.._................_..._.."__-_....._..._...._........._...._..._................ <br />NONCHLOR. SOLVTS <br />_..__...._.___._..._..,.... <br />-_. <br />_ .....__..... ,.,_.... _........... <br />WASTE/USED OIL <br />..... _._................. .__... <br />MINIMUM VERIFICATION LABORATORY ANALYSES TERMINOLOGY <br />The following listing of <br />terminology used. will be <br />laborator analyses abbreviations is provided as a guide so <br />more familiar. <br />that <br />described in EPA SW 846, <br />All analyses methods are designated EPA methods as <br />Third Edition. Those methods not found in SW 846, <br />specifically noted. <br />are <br />TPH G <br />TPH D <br />Total Petroleum Hydrocarbon, Gasoline <br />TEPH <br />Total Petroleum Hydrocarbon, Diesel <br />BTX & E (8020) <br />Total Extractable Petroleum Hydrocarbon (8015) <br />Benzene, Toluene, Xylene & Ethyl Benzene (8020) <br />CL HC 8010 OR 8240 <br />TEL (DOHS-LUFT) <br />ChlorinatedHydrocarbon 8010 or 8240 <br />Tetraethyl Lead (DOHS-LUFT) <br />EDB (DOHS -AB 1803) <br />GC FID <br />Ethylene dibromide (DOHS -AB 1803) <br />ICP -AES OR AA <br />Gas Chromatography Flame Ionization Detector <br />Inductively Coupled Plasma Atomic Emission Spectrometry or Atomic <br />Method 5030 <br />Method 3550 <br />Spectrometry <br />Purge and Trap Sample Preparation <br />Method <br />Method 3540 <br />QA/QCQuality <br />Sonication Sample Preparation <br />Soxhlet Sample Pre ration <br />Assurance/Quality Control <br />Notes: To avoid false positive detectionofbenzene, benzene -free solvents are to be used. <br />"firstused ccut"l2hc"dirty"are <br />column be <br />proper QA/QC is followed. <br />samplese ore once theked hydrocarbonsahavekbeencharacterized sandas a <br />organicsFor be uusedkingprefereer <br />for larellower <br />nce tostheP600esermesdbecausetthe5detection <br />the QA/QC is better. <br />liimitsies <br />and <br />SITE ADDRESS <br />SWEEPS # <br />CONTRACTOR APPROVAL DATE <br />