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Job Narrative <br /> 720-26649-2 <br /> Comments <br /> No additional comments. <br /> Receipt <br /> All samples were received in good condition within temperature requirements. <br /> GC Semi VOA <br /> Method 80156:The matrix spike/matrix spike duplicate(MS/MSD)precision for batch 70112 was outside control limits. <br /> Non-homogeneity of the sample matrix is suspected. The associated laboratory control sample/laboratory control sample duplicate <br /> (LCS/LCSD)precision met acceptance criteria. <br /> Method 80156:Due to the level of dilution required for the following sample,surrogate recoveries are not reported:HA-5-1 (720-26649-9). <br /> Method 80156:The following sample(s)was analyzed outside the method defined holding time because the request for the test was <br /> made after the holding time for the sample expired: HA-1-1 (720-26649-1), HA-2-1 (720-26649-3), HA-3-1 (720-26649-5), HA-3-3 <br /> (720-26649-6), HA-4-1 (720-26649-7), HA-4-3(720-26649-8), HA-5-1 (720-26649-9), HA-5-3(720-26649-10), HA-6-1 (720-26649-11), <br /> HA-6-3(720-26649-12), HA-1-3(720-26649-2), HA-5-1 (720-26649-9). <br /> Method 80156:Due to the level of dilution required for the following sample,surrogate recoveries are not reported: HA-5-1 (720-26649-9), <br /> HA-6-1 (720-26649-11). <br /> Method 801513:Capric acid surrogate recovery for the following sample was outside control limits: HA-1-3(720-26649-2), HA-5-3 <br /> (720-26649-10). Evidence of matrix interference is present;therefore, re-extraction and/or re-analysis was not performed. <br /> No other analytical or quality issues were noted. <br /> Organic Prep <br /> No analytical or quality issues were noted. <br /> Page 2 of 44 <br />