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Y <br /> Matrix Spike Recoveries <br /> EPA 8141A OP Pesticides Soil RECEIVED <br /> OCT 15 2001 <br /> APPL Inc. <br /> APPL ID: 010917S-22107 MS .40017 4203 West Swift Avenue <br /> BatchlD: $8141S-0109178 <br /> Fresno, CA 93722 <br /> Compound Name Spike Lvl Matrix Result SPK Result DUP Result SPK% DUP % Recovery RPD RPD <br /> ug/kg ug/kg ug/kg ug/kg Recovery Recovery Limits % Limits <br /> Coumaphos 417 ND 457 451 110 108 46-140 1.3 30 <br /> 104# 20-101 11.0 30 <br /> Demeton (Total) 83.3 ND 77.4 86.4 92.9 <br /> Dichlorvos 83.3 ND 93.2 93.8 112 113 29-145 0.64 30 <br /> Disulfoton 83.3 ND 78.7 82.3 94.5 98.8 37-116 4.5 30 <br /> EPN 83.3 ND 108 103 130 124 28-196 4.7 30 <br /> Ethion 83.3 ND 88.6 85.1 106 102 54-121 4.0 30 <br /> Fensulfothion 417 ND 498 477 119 114 26-177 4.3 30 <br /> Fenthion 83.3 ND 86.6 85.2 104 102 41-126 1.6 30 <br /> Malathion 83.3 ND 96.3 94.4 116 113 49-129 2.0 30 <br /> Parathion, ethyl <br /> 83.3 ND 92.3 90.7 111 109 28-167 1.7 30 <br /> Ronnel 83.3 ND 86.0 86.1 103 103 47-120 0.12 30 <br /> Stirophos <br /> 167 ND 210 207 126 124 43-154 1.4 30 <br /> Sulfotep 83.3 ND 87.5 89.5 105 107 52-123 2.3 30 <br /> Trichloronate 83.3 ND 86.7 90.5 104 109 41-138 4.3 30 <br /> Surrogate:Tri butylphosphate 167 NA 180 183 108 110 41-142 <br /> Surrogate:Triphenylphosphate 167 NA 168 161 101 96.4 41-137 <br /> #= Recovery is outside QC limits. <br /> Comments: <br /> �iI Prima SPK DUP <br /> Extraction Date : 9/17/01 9/17/01 <br /> Analysis Date : 9119/01 9/19/01 <br /> I Instrument: NP003 NPD03 <br /> Run : 73 74 <br /> Analyst: KW <br /> �� Printed. 9124/01 2:13:33 PM <br />