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d-15-1997 2: 1APM FROM ENGEO INC 510 838 7d25 P- 14 APR-I1-97 FRI 12:32 AEN CALIK dA FAX NO. 5109300256 P. 18/27 NAGE 14 ENGEO INCORPORATED SAMPLE ID: 80-1 DATE SAMPLED: 03/31/97 AEN LAB NO: 9704016-05 DATE RECEIVED: 04/01/97 AEN WORK ORDER: 9704016 REPORT DATE: 04/11/97 CLIENT PROJ. ID: 420342 METHOD/ REPORTING DATE ANALYTE CAS# RESULT LIMIT UNITS ANALYZED #Digestion. Metals by GFAA EPA 3050 Prep Date 04/08/97 #Digestion. Metals AA/ICP EPA 3050 Prep Date 04/08/97 #Extraction for Pest/PCBs EPA 3550 Extrn Date 04/07/97 Pesticides & PCBs EPA 8080 Aldrin 309-00-2 ND 5 U91K9 04/09/97 alpha-BIIC 319-84-6 NO 5 ug/kg 04/09/97 beta-BHC 319-85.7 NO 5 ug/kg 04/09/97 delta-BHC 319-86.8 NO 5 uy/kg 04/09/97 gamma-BHC (Lindane) 58-89-9 ND 5 ug/kg 04/09/97 Chlordane 57-74-9 NO 50 ug/kg 04/09/97 4.4' -DDD 72-54.8 ND 10 ug/kg 04/09/97 2.4* -DDD 53-19-0 NO 10 ug/kg 04/09/97 4.4' -ODE 72 55-9 ND 10 ug/kg 04/09/97 2.4' -DDE 3424.82-6 ND 10 ug/kg 04/09/97 4,4' -OOT 50-29-3 NO 10 ug/kg 04/09/97 2.4' -DDT 789-02-6 ND 10 ug/kg U4/09/97 Dieldn n 60-57-1 NO 10 ug/kg 04/09/97 Endosuifan 1 959-98-8 ND 5 ug/kg 04/09/97 Endosulfan 11 33212-65.9 ND 1G u9/k9 04/09/97 Endosulfan Sulfate 1031-07 8 NO 10 u9/kg 04/09/97 Endrin 72-20.8 NO 10 ug/kg 04/09/97 Endrin Aldehyde 7421.93-4 NU 10 ug/kg 04/09/97 Heptachlor 76-44-8 NO 5 ug/kg 04/09/97 Hentacnior Epoxide 1024-57-3 NO 5 ug/kg 04/09/97 Methoxychlor 72-43.5 NO 10 u9/kg 04/09/97 Toxaphene 8001-35.2 ND 5U uq/kq 04/09/97 Armlur 1016 12674-11 2 NO 50 ug/kg 04/09/97 Aroclor 1221 11104-28-2 NO 50 ug/kg 04/09/97 Aroclor 1232 1.1141-16-5 NO 50 ug/kg 04/09/97 Aroclor 1242 53469-21.9 NO 50 ug/kg 04/U9/97 Aroclor 1248 12672.29-6 NO 60 ug/kg 04/09/97 Aroclor 1254 11097.69.1 NO 50 ug/kg 04/09/97 Aroclor 1260 11096-82-5 NO 50 uq/Kg 04/09/97 CCR 17 Metals Silver EPA 6010 0.1 ' 0.1 mg/kg 04/09/97 Arsenic EPA 7060 1 3 * 0.5 mg/kg 04/09/97 Barium EPA 6010 89 * 1 mg/kg 04/09/97 Beryllicun EPA 6010 0.2 * 0.1 mg/kg 04/09/97