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PAGE 13 ENGEO INCORPORATED SAMPLE ID: 6-4 DATE SAMPLED: 11/27/96 AEN LAB N0: 9611399.09 DATE RECEIVED: 11/27/96 AEN WORK ORDER: 9611399 REPORT DATE: 12/11/96 CLIENT PROD. ID: 4203-F2 METHOD/ REPORTING DATE ANALYTE CAS$ RESULT LIMIT UNITS ANALYZED Vinyl Acetate 108-05-4 ND 50 ug/kg 12/05/96 Vinyl Chloride 75-01-4 NO 10 ug/kg 12/05/96 Xylenes Total 1330-20-7 ND 10 ug/kg 12/05/96 #Extraction for Pest/PCBs EPA 3550 Extrn Date 12/06/96 Pesticides & PCBs EPA 8080 Aldrin 309-00-2 ND 10 ug/Kg 12/09/96 alpha-BHC 319-84-6 ND 10 ug/Kg 12/09/96 beta-BHC 319-85-7 ND 10 ug/Kg 12/09/96 delta-BHC 319-86-8 ND 10 ug/Kg 12/09/96 gamma-BHC (Lindane) 58-89-9 ND 10 ug/Kg 12/09/96 Chlordane 57-74-9 ND 100 ug/Kg 12/09/96 4,4'-DDD 72-54-8 ND 20 ug/Kg 12/09/96 2,4' -DDD 53-19-0 ND 20 ug/Kg 12/09/96 4,4'-DDE 72-66 9 NO 20 ug/Kg 12/09/96 2.4'-DDE 3424-82-6 ND 20 ug/Kg 12/09/96 4,4'-DDT 50-29-3 ND 20 ug/Kg 12/09/96 2.4'-DDT 789-02-6 ND 20 ug/Kg 12109/96 Dieldrin 60-57-1 ND 20 Ug/Kg 12/09/96 Endosulfan 1 959-98-8 ND 1.0 ug/Kg 12109/96 Endosulfan 11 33212-65-9 ND 20 ug/Kg 12/09/96 Endosulfan Sulfate 1031-07-8 NO 20 ug/Kg 12/09/96 Endrin 72-20-6 ND 20 ug/Kg 12/09/96 Endrin Aldehyde /421-93-4 NO 20 ug/Kg 12/09/96 Heptachlor 76-44-8 N0 10 ug/Kg 12/09/96 Heptachlor Epoxide 1024-57-3 ND 10 ug/Kg 12/09/96 Methoxychlor 72-43-5 ND 20 ug/Kg 12/09/95 toxaphene 8001-35-2 NO 100 ug/Kg 12/09/96 Aroclor 1016 12674-11-2 NO 100 ug/Kg 12/0919b Aroclor 1221 11104-28-2 ND 100 ug/Kg 12/09/96 Aroclor 1232 11141-16-5 ND 100 ug/Kg 12/09/96 Aroclor 1242 53469-21-9 ND 100 ug/Kg 12/09/96 Aroclor 1248 12672-29-6 NO 100 ug/Kg 12/09/96 Aroclor 1254 11097-69-1. NO 100 ug/Kg 12/09/96 Aroclor 1260 11096-82-5 NO 100 ug/Kg 1Z/09/96 CCR 17 Metals Silver EPA 6010 NO 0.1 mg/kg 12/09/96 Arsenic EPA 7060 1.6 * 0.5 mg/kg 12/08/96 BarirIiU11 EPA 6010 85 Beryl * 1 mg/kg 12/09/96 Cadium EPA 6010 ND 0.1 mg/kg 12/09/96 EPA 6010 ND 0.2 mg/kg 12/09/96 ZC/E1 'd 9520 £0 6015 'ON Sd.d d1N60.jIlV0)d9 11:L1 03N 96-11-030