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. 1534 WiIIow Pass Road,Pittsburg,CA 94565-1701 <br /> McCam obeli Analytical. Inc <br /> Web:www.mccampbehcom E-mail:main@mccampbeltanon <br /> "When Ouality Counts" Tele hone:877-252-9262 F. 925-252-9269 <br /> Safety Kleen Client Project ID: Sample A;Wast Ink Date Sampled: 09/19/08 <br /> 5050 Salida Blvd Date Received: 09/23/08 <br /> Client Contact: Jason Flores Date Extracted: 09/25/08-09/29/08 <br /> Salida,CA 95368 Client P.O.: Date Analyzed 09/25/08-09/29/08 <br /> CA Title 22 Acute Fish Bioassay Screen Test for Hazardous Waste <br /> Extraction Method: CA DFG(Polinsi&Miller) Analytical Method: CADFG(Polinsi&Miller) Work Order: 0809678 <br /> Lab ID 0809678-002A Species Pimephales promelas Avg.Length(mm) 36.9 <br /> Client ID Sample B Common Name Fathead Minnows Aviv.Weight(g) I 0.339 <br /> Matrix Solid Max Weight(e) 0.346 <br /> Control Water Moderately Hard Syn Min Weigh[ g) 0.331 <br /> Survival Dissolved 02(mg/L) pH Temperature(cQ <br /> Concentration Comments <br /> A B A B A B A B <br /> Control 10 10 7.89 7.95 7.30 7.31 19.8 19.8 Analyst: CM <br /> 250 mg/L 10 10 7.91 7.95 7.20 7.17 19.8 19.8 <br /> 500 mg/L 10 10 7.91 7.98 7.15 7.16 19.8 19.8 Date: 9/25/2008 <br /> 750 mg/L 10 10 7.90 7.95 7.16 7.15 19.8 19.8 Time: 11:00 AM <br /> Control 10 10 7.67 7.75 7.26 7.25 19.9 19.9 Analyst: C M <br /> 250 mA/L 10 10 6.19 6.09 7.11 7.10 19.9 19.9 <br /> 500 mg/L 10 10 6.11 6.05 7.09 7.08 19.9 19.9 Date: 9/26/2008 <br /> 750 mg/L 10 10 5.91 6.10 7.05 7.02 19.9 1 19.9 Time: 11:00 AM <br /> Control 10 10 7.52 7.48 7.46 1 7.43 19.8 1 19.8 Analyst C M <br /> 250 mg/L 10 10 7.60 7.55 7.07 7.05 19.8 19.8 <br /> 500 mg/L 10 10 7.40 7.40 7.10 7.09 19.8 19.8 Date: 9/27/2008 <br /> 750 mg/L 10 10 7.00 7.01 T11 7.10 19.8 19.8 Time: 11:00 AM <br /> Control 10 10 T14 7.22 T24 7.27 19.9 19.9 Analyst: CM <br /> 250 mg/L 10 10 6.78 6.81 7.27 7.23 19.9 19.9 <br /> 500 mg/L 10 10 6.84 6.79 7.28 7.25 19.9 19.9 Date: 9/28/2008 <br /> 750 mg/L 10 10 6.67 6.58 7.24 7.24 19.9 19.9 Time: 11:00 AM <br /> Control 10 10 6.98 7.13 7.34 7.36 19.8 19.8 Analyst: C M <br /> 250 mg/L 10 10 6.30 6.77 7.26 7.21 19.8 19.8 <br /> 500 mg/L 10 10 6.55 6.61 7.22 7,20 19.8 19.8 Date: 9/29/2008 <br /> 750 mg/L 10 10 6.48 6.59 7.20 7.19 19.8 19.8 Time: 11:00 AM <br /> Initial Fina) <br /> Control 750 m Control 750 m <br /> Hardness m as CaCO3 44 48 44 50 <br /> Alkalin m as CaCO3 34.32 34.6 35 34.04 <br /> Conductivity uS/em) 184.8 179.3 198.4 184 <br /> Salim m N/A N/A N/A N/A <br /> Result:Mortality<40%at 750me/L. Therefore LC50>=500m /L('non-hazardous') <br /> 96 LC50: N/A LC50 Method: N/A <br /> 95%Upper Confident Limit: N/A 95%Lower Confident Limit: N/A <br /> DHS ELAP Certification 1644 Angela Rydelius,Lab Manager <br />