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AOL <br /> MCCampbell Analytical, Inc. 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> Web:www.mccampbek.com E-mail:meio(a3nccamp6ell.com <br /> "When Ouelim Counts" Telephone 877-252-9262 Fax:925-252-9269 <br /> QC SUMMARY REPORT FOR SM5210B <br /> W.O.Sample Matrix: Liquid QC Matrix: Water BatchlD: 38439 WorkOrder 0809678 <br /> EPA Method SM6210B Extraction SM5210B Spiked Sample ID: WA <br /> Sample Spiked MS I MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(°k) <br /> Analyte <br /> mg/L mg/l- %Rec. %Rec. %RPD %Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> BOD N/A` 198 N/A N/A I N/A 1 98.2 98.5 1 0.257 1 N/A I N/A 1 80- 120 1 16 <br /> All target compounds in the Method Blank of this extraction batch were NO less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 38439 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0809678-001A 09/19/08 10:30 AM 09/29/08 10/06/08 1:56 PM <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)12). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification 1644 .—QA/Q'- '�Tcer <br />