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March 23, 2009 Lab 1D : STK0932215 Proactive Customer : 3-16551 Quality Control - Inorganic Constituent Method Date/1D Ty pc Units Cone. QC Data DQO Note Metals silver 6010B 03/20/2009:203583 CCB ppm 0.00005 0.01 CCV ppm 0.9990 100% 90-110 CCB PPM 0.00007 0.01 halhum 6010B 03/20/2009:203583 CCV ppm 0.9990 100% 90-110 CCB ppm 0.0048 0.01 CCV ppm 0.9990 100% 90-110 CCB PPM -0.0005 0.01 l'anadium 6010B 0320/2009:203583 CCV ppm 0.9990 101% 90-110 CCB ppm 0.000009 0.01 CCV ppm 0.9990 101% 90-110 CCB PPM -0.00002 0.01 60108 03/20/2009:203583 CCV ppm 0.9990 101% 90-110 CCB ppm -0.0004 0.02 CCV ppm 0.9990 100% 90-110 CCB PPM -0.0005 0.02 V1crcu5 7470 03113/2009:202654 Blank ug/L ND <0.02 LCS ug/L 0.2000 89.5% 85-115 MS ug/L 0.2000 85.8% 75-125 (SP 0902348-001) MSD ug/L 0.2000 91.3% 75-125 MSRPD ug/L 0.2000 5.9% _<20 7470 03/23/2009:202991 Blank mg/kg ND <0.03 LCS mg/kg 0.2500 94.8% 85-115 MS mg/kg 0.2500 78.6% 75-125 (SP 0902478-001) MSD mg/kg 0.2500 58.8% 75-125 435 MSRPD inWkg 0.2500 8.9% <20 Wet Chem Solids,Suspended 2540D 03/12/2009:300195 Blank mg/L ND LCS mg/L 500.0 100% 38-138 LCS mg/L 500.0 99.4% 38-138 Dun I mg/L I 0.4% 28.7 /o Solids 2540E 03/122009:202609 Blank % ND <0.1 Du % 0.1% 23.9 PH 4500HB 03/12/2009:203206 CCV units 8.000 100% 95-105 CCV units 8.000 100% 95-105 BOD 5210B 03111/2009:202575 RgBlk mg/L 0.82 2 b RgBlk mg/L 0.23 2 b LCS mg/L 197.4 91.5% 60-120 Dup mg/L 11.5% 15.9 Dup m 7.4% 15.9 52108 03,/11/2009:202577 RgBlk mg/L 0.47 2 b RgBlk mg/L 0.25 2 b LCS mg/L 197.4 111% 60-120 LCS mg/L 197.4 104% 60-120 Dup ing/L 79.0% 15.9 440 Dup mg/L 13.1% 15.9 Dup mg/L 21.5% 1 15.9 440 5210B 03/11/2009:202578 RgBlk mg/kg 0.18 2 RgBlk mg/kg 0.11 2 LCS mg/kg 197.4 101% 60-120 LCS mg/kg 197.4 99.4% 60-120 Dup mg/kg 4.7% 15.9 loop 1m /k 19.9% 15.9 440 5210B 03116/2009:203194 CCV mg/L 1.000 103% 80-120 CCV m L L000 103% 80-120 Page 22 of 23