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• �tCEIVfi� <br /> FEB 2 4 2015 <br /> CASTLE ANALYTICAL LABORATORY cn1V1R0NMENTAL <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater, C Qiru nl-v Phone (209)384-2930 <br /> Certificate#2480 Fax: (209)384-1507 <br /> George W. Lowry, Inc. Client Project ID: Pacific Southwest Irrigation Method: EPA 5030/8260B <br /> P.O. Box 176 Lab Reference Number: 1502005 Instrument ID:VARIAN MS <br /> Salida,CA 95368 Sample Description:Soil Prepared: 02-03-15 <br /> Attn: Colin Kelley Sample Prep/Analysis Method: EPA 5030/8260 Analyzed: 02-03-15 <br /> Reported: 02-10-15 <br /> QUALITY CONTROL DATA REPORT <br /> SPIKE ID: VSMS-2035 ME <br /> Reporting BLANK Spiking Control %R <br /> Limit Result Level Spike Limits <br /> mg/Kg mg/Kg mg/Kg %R <br /> COMPOUNDS <br /> --- <br /> t-But,IAlcohol t-BA) 0.80 ND 3.0NA' ---70-1 30 <br /> Methyl t-but I ether (MTBE) 0.020 ND 0.10 NA- 70-130 <br /> Diiso ro I ether DIPE) 0.020 ND 0.10 NA* 70-130 <br /> Ethyl -Butyl ether(ETRE 0.020 ND 0.10 NA* 70-130 <br /> t-Am I meth I ether(TAME 0.020 ND 0.10 NA* 70-130 <br /> 12ichloroethane 1,2-DCA) 0.020 ND 0.10 NA' 70-130 <br /> glene dibromide(EDB) 0.020 ND 0.10 NA* 70-130 <br /> 1,1-Dlchloroethene(1,1,DCE) 0.020 NO 0.10 NA• 70-130 <br /> Benzene 0.020 ND 0.10NA* ---T0-1 30 <br /> Trichloroethene(TC E) 0.020 ND 0.10 NA* 70-130 <br /> Toluene 0.020 ND 0.10 NA* 70-130 <br /> Chlorobenzene 0.020 ND 0.10 NA' 70-130 <br /> Surro ate: <br /> Dibromofluoromethane 0.40 ---9'52% 0.40 NA* fu-130 <br /> 1,2-Dichloroethane-d4 0.40 98.3% 0.40 NA* 70-130 <br /> Toluene-d8 0.40 85.3% 0.40 NA* 70-130 <br /> 4-Bromofluorobenzene 0.40 108% 0.40 NA' 70-130 <br /> Spiking CONTROL CONTROL %R %RPD <br /> Level SPIKE SPIKE DUP Limits <br /> mg/Kg %R %R <br /> COMPOUNDS o 10.6% <br /> t-But I Alcohol t-BA) 3.0 99.4% 89.4% 60-130% <br /> Meth I t-but I ether (MTBE) 0.10 102% 102% 70-130% 0.00% <br /> Diisopro lether(DIPE 0.10 103% 101% 70-130% 2.35% <br /> Eth I t-But I ether(ETBE) 0.10 98.0% 101% 70-130% 2.82% <br /> t-Am I meth I ether(TAME 0.10 93.6% 98.4% 70-130% 5.00% <br /> 1,2-Dichloroethane(1,2-DCA) 0.10 93.6% 94.0% 70-130% 0.426% <br /> Eth lene dibromide(EDB) 0.10 94.8% 102% 70-130% 6.92% <br /> 1,1-Dichloroethene(1,1,DCE 0.10 65.2% 68.8% 60-130% 5.37% <br /> Benzene 0.10 89.6% 92.0% 70-130% 2.64% <br /> Trichloroethene(TCE) 0.10 87.2% 92.0% 70-130% 5.36% <br /> Toluene 0.10 88.8% 90.8% 70-130% 2.23% <br /> Chlorobenzene 0.10 91.6% 96.4% 70-130% 5.11% <br /> Surro ate: <br /> Dibromofluoromethane 0.40 117% 95.1% 70-130% 21.0% <br /> 1,2-Dichloroethane-d4 0.40 123% 93.3% 70-130% 27.2% <br /> Toluene-d8 0.40 106% 84.3% 70-130% 23.1% • <br /> 4-Bromofluorobenzene 0.40 118% 92.1% 70-130% 25.0% <br /> 'See Control Spike/Control Spike Duplicate <br /> APPROVED BY: <br /> James C. Phillip / aboratory Director or <br /> Clari J. Cone/ aboratory Manager <br />