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1534 Tallon Pass Road,52.92621 CA 94555.1701 <br /> McCampbell Analytical, Inc. Toil Free ,nCG Pb:(877)32.9 n"inr:(923)252.9259 <br /> huplAvmv.mcemnp6ell.coinIa-moil:nwinQmccempbelLrnm <br /> "When Quality Counts" ' <br /> Quality Control Report <br /> ECEtVE� <br /> Client: Castle Analytical Laboratory WorkOrder: 1502090 <br /> Date Prepared: 2/4/15 BatchlD: 100763 APR 08 2015 <br /> Date Analyzed: 214/15 Extraction Method: SW3550B ENVIRONMENTAL <br /> Instrument: GC21 Analytical Method: SW9270C ENTAL <br /> Matrix: Soil Unit: mg/Kg I��A 1rjFDdD?4�c�T <br /> Project: #1502005/Pacific Southwest Irrigation Sample ID: MB/LCS-100763 <br /> 1502047-00 t AMS/MSD <br /> QC Summary Report for SW8270C <br /> Analyte MB LCS RL SPK MB SS LCS LCs <br /> Result Result Val %REC %REC Limits <br /> Dl-n-octyl Phthalate ND - 0.50 - - - <br /> 1,2-Diphenylhydrazine ND - 0.25 - - <br /> Fluoranthene ND - 0.25 - - - - <br /> Fluorene ND - 0.25 - - - <br /> Hexachlorobenzene ND - 0.25 - - - - <br /> Hexachiorobutodiene ND - 0.25 - - - <br /> Hexachlorocyclopentadiene ND - 1.3 <br /> Hexachloroethane ND - 0• - - <br /> Indeno(1,2,3•cd)pyrene ND - 0.25 - - - - <br /> rone ND - 0.25 <br /> 2-Meth - - <br /> 2•Methylnaphthalene ND 0.25 <br /> 2-Methyiphenol(o-Cresol) ND 0.25 <br /> Naphihalene ND 0.25 <br /> 2-1,11troaniline ND - 1.3 - - - <br /> 3-Nltroanillne ND - 1.3 - - <br /> 4-Nllroaniline ND - 1.3 - <br /> Nilrobenzere ND - 0.25 - - - <br /> 2-1,111rophenol ND - 1.3 - - <br /> 4-Nilrophenol ND 3.91 1.3 5 - 78 30-130 <br /> N-Nilrosodiphenylamine ND - - 0.25 - - - - <br /> N-Nibosodi-n-propylamine ND 3.82 0.25 5 - 76 30-130 <br /> Pentachlorophenol ND 4.52 1.3 5 - 90 30430 <br /> Phenanthrene ND - 0.25 - - - - <br /> Phenol ND 4.71 0.25 5 - 94 30-130 <br /> Pyrene ND 4.58 0.25 5 - 92 30-130 <br /> 1,2,4Tdchlombenzene ND 6.12 0.25 5 - 102 30-130 <br /> 2,4,5-Trichlorophenol ND - 0.25 - - - - <br /> 2,4,6-Trichlorophenol ND - 0.25 - - - <br /> Surrogate Recovery . <br /> 2-Fluorophenot 5.22 4.B5 5 104 97 30-130 <br /> Phenol-d5 - 5.14 4.36 5 103 87 30-130 <br /> Nitrobenzene-d5 4.42 4.51 5 08 90 30.130 <br /> 2-Fluorobiphenyl 4.49 4.54 5 90 93 30.130 <br /> 2,4,6-Tribromophenal 2.31 2.71 5 46 54 10-1311 <br /> 4-Terphenyl•d14 4.33 4.44 5 87 89 30-130 <br /> (Cont.) " <br /> CDPH ELAP 1644 f NELAP 4033ORELAP <br /> ' QA/QCOfficer <br /> Page S of N <br /> r <br />