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0 0 MATRIX SPIKE SAMPLE EVALUATION REPORT TOTAL Metals Client Lot #. . . : D6I060141 Matrix. ..... . . .: WATER Date Sampled. . . : 09/05/06 10:15 Date Received. . : 09/06/06 PERCENT RECOVERY RPD PREPARATION- WORK PARAMETER RECOVERY LIMITS RPD LIMITS METHOD ANALYSIS DATE ORDER # Copper 108 (82 - 129) SW846 6010B 09/12-09/13/06 JDQ361CP 104 (82 - 129) 3.3 (0-25) SW846 6010B 09/12-09/13/06 JD0361CQ Dilution Factor: 1 Analysis Time.. : 19:12 Nickel 103 (84 - 120) SW846 6010B 09/12-09/13/06 JDQ361CR 99 (84 - 120) 4.1 (0-25) SW846 6010B 09/12-09/13/06 JDQ361CT Dilution Factor: 1 Analysis Time.. : 19:12 Lead 104 (89 - 121) SW846 6010B 09/12-09/13/06 JDQ361CU 100 (89 - 121) 4.2 (0-25) SW846 6010B 09/12-09/13/06 JDQ361CV Dilution Factor: 1 Analysis Time.. : 19:12 Antimonl 113 (81 - 124) SW846 6010B 09/12-09/13/06 TDQ361CW 111 (81 - 124) 1.6 (0-25) SW846 6010B 09/12-09/13/06 JDQ361CX Dilution Factor: 1 Analysis Time..: 19:12 Seleniufo 104 (71 - 140) SW846 6010B 09/12-09/13/06 JDQ361CO 100 (71 - 140) 4.0 (0-25) SW846 6010B 09/12-09/13/06 JDQ361CI Dilution Factor: 1 Analysis Time..: 19:12 Thallium 105 (90 - 116) SW846 601013 09/12-09/13/06 JDQ361C2 101 (90 - 116) 4.1 (0-25) SW846 6010B 09/12-09/13/06 JDQ361C3 Dilution Factor: i Analysis Time.. : 19:12 Vanadium 104 (85 - 120) SW846 6010B 09/12-09/13/06 TDQ36lC4 99 (85 - 120) 4.1 (0-25) SW846 6010B 09/12-09/13/06 JDQ361C5 Dilution Factor. 1 Analysis Time..: 19:12 Zinc 100 (60 - 137) SW846 6010B 09/12-09/13/06 JDQ361C6 97 (60 - 137) 2.9 (0-25) SW846 6010B 09/12-09/13/06 JDQ361C7 Dilution Factor: 1 Analysis Time..: 19:12 Molybdenum 108 (83 - 109) SW846 6010B 09/12-09/13/06 JDQ361C8 106 (83 - 109) 1.9 (0-25) SW846 6010E 09/12-09/13/06 JDQ361C9 Dilution Factor: 1 Analysis Time..: 19:12 NOTE(S) : Calculations are performed before rounding m avoid round-off errors in calodated rewha.