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01 • <br /> Client: Stockton Scavengers Association Inc QC Sample Results TestAmerica Job ID: 280-41009-2 <br /> Project/Site: CA10021Stockton Scavengers <br /> ........_..................... <br /> Method: 8260B --Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: 280.40931-A-2-A MS Client Sample ID: Matrix Spike <br /> Matrix:Solid Prep Type:TCLP <br /> Analysis Batch: 170430 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Chloro benzene ND 0.0500 0.0502 mgM911- 100 78-135 <br /> be <br /> Chloroform ND 0.0500 0.0535 mg/L 107 76-120 _ <br /> 1,2-Dichloroethane ND 0.0500 0.0512 mglL 102 70-135 <br /> 1,1-Dichloroelhene ND 0.0500 0.0644 mg/L 129 71-138 <br /> Tetrachloroethene ND 0.0500 0.0537 mg/L 107 70-135 <br /> Trichloroethene ND 0.0500 0.0523 mg/L 105 73-135 <br /> Vinyl chloride ND 0.0500 0.0565 mg/L 113 40.144 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> 1,2-Dichloroethaned4(Sum) 101 64-129 <br /> Toluene-d8(Surr) 100 78-120 <br /> 4-Bromofluorobenzene(Sun) 105 78-121 <br /> Dibromotluoromethane(Sun) 108 79-119 <br /> Lab Sample ID: 280.40931-A-2-A MSD Client Sample ID: Matrix Spike Duplicate <br /> Matrix: Solid Prep Type:TCLP <br /> Analysis Batch: 170430 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Benzene 0.0049 J 0,0500 0.0551 mg 100 74-135 5 20 <br /> 2-Butanone(MEK) 0.20 0.200 0.426 mg/L 114 44.150 4 32 <br /> Carbon tetrachloride ND 0.0500 0.0508 mg/L 102 67-135 9 21 <br /> Chlorobenzene ND 0.0500 0.0477 mg/L 95 76-135 5 20 <br /> Chloroform ND 0.0500 0.0500 mg/L 100 76.120 7 20 <br /> 1,2-Dichloroethane ND 0.0500 0.0483 mg/L 97 70-135 6 20 <br /> 1,1-Dichloroethene ND 0.0500 0.0626 mg/L 125 71-136 3 20 <br /> Tetrachloroethene ND 0.0500 0.0517 mg/L 103 70-135 4 20 <br /> Trichloroethene ND 0.0500 0.0495 mg/L 99 73-136 6 20 <br /> Vinyl chloride ND 0.0500 0.0549 mg/L 110 40-144 3 24 <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits <br /> 1,2-Dich1oroethaned4(Sum) 97 64-129 <br /> Toluenad8(Sura 100 78-120 <br /> 4-Bromolluorobenzene(Sum) 105 78-121 <br /> Dibromofluoromethane(Sum) 105 79-119 <br /> ....... ...... <br /> Method: 6010B -Metals (ICP) <br /> Lab Sample ID: LB 320-14761/1-A ^10 LB Client Sample ID: Method Blank <br /> Matrix: Solid Prep Type: STLC Citrate <br /> Analysis Batch: 15063 <br /> LB LB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac <br /> a-- ND 0.10 0.0042 mg/L 04/24/1322:08 10 <br /> Arsenic ND 0,20 0.12 mg/L 04/24/1322:08 10 <br /> Barium ND 0.10 0.020 mg/L 04/24/1322:08 10 <br /> Beryllium 0.00220 J 0.050 0.0015 mg/L 04/24/13 22:08 10 <br /> TestAmerica Denver <br /> Page 11 of 20 5/3/2013 <br />