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GeoAnalytical Laboratories, Inc. 2300 Maryann Dr. Turlock,CA 95380 Phonc(209)669-0100 Fax(209)593-2212 email: infooageoanalyticallab.com Report# A4B2104 Date: 03/12/14 San Joaquin County Environmental Health Date Recd: 02/21/14 1868 East Hazelton Ave Stockton,CA 95205 Inorganic Chemistry- Quality Control GeoAnalytical Laboratories, Inc. Reporting Spike Source %REC RPD 11\na1%tC Result Limit Units Level Result %REC Limits RPD [,unit Notes Batch A000531 -3050B Prepared & Analyzed: 02/27/14 LCS Dup(A000531-BSD 1) Antimony 3.28 0.5 mg/kg 3.125 105 80-120 4 20 Arsenic 6.30 0.5 6.250 101 80-120 4 20 Barturn 13.5 0.5 12.50 108 80-120 4 20 Beryllium 3.05 0.5 3.125 97 80-120 3 20 Cadmium 6.25 0.5 6.250 100 80-120 2 20 Chromium 13.7 0.5 12.50 109 80-120 2 20 Cobalt 13.3 0.5 12.50 107 80-120 2 20 Copper 14.2 0.5 12.50 113 80-120 0.07 20 Lead 12.6 1.0 12.50 101 80-120 0.5 20 Molybdenum 3.10 0.2 3.125 99 80-120 2 20 Nickel 13.3 0.5 12.50 106 80-120 5 20 Selenium 5.93 0.5 6.250 95 80-120 0.8 20 Silver 6.20 1.0 6.250 99 80-120 0.6 20 thallium 3.61 0.5 3.125 116 80-120 0.5 20 Vanadium 6.71 0.5 6.250 107 80-120 8 20 Zinc 12.5 0.5 12.50 100 80-120 2 20 Mercury 0.52 0.5 0.6250 82 80-120 0.4 20 Matrix Spike(A000531-MSI) Source:A4B1_312-01 Antimony 84,3 0.5 mg/kg 3.125 81.7 82 80-120 Arsenic 6.02 0.5 6.250 ND 96 80-120 Barium 57.7 0.5 12.50 43.7 111 80-120 Heryllium 3.17 0.5 3.125 ND 101 80-120 Cadmium 10.9 0.5 6.250 4.62 101 80-120 Chromium 59.4 0.5 12.50 48.7 86 80-120 Cobalt 18.0 0.5 12.50 5.13 103 80-120 Copper 2110 0.5 1250 1730 NR 80-120 QM-(2 Lead 94.5 1.0 12.50 74.8 158 80-120 QM-(2 Molybdenum 36.2 0.2 3.125 32.9 103 80-120 Nickel 50.7 0.5 12.50 37.2 108 80-120 Selenium 5.47 0.5 6.250 ND 88 80-120 Silver 6.92 1.0 6.250 7.09 NR 80-120 QM-(,1 'thallium 2.25 0.5 3.125 ND 72 80-120 QM-(.I Vanadium 9.17 0.5 6.250 2.82 102 80-120 Zinc 681 0.5 12.50 668 106 80-120 Mercury 0.70 0.5 0.6250 ND 112 80-120 Certification#2585