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April 14, 2004 Lab ID : STK431922 Valley Industries Customer : 3-11146 Quality Control - Inorganic Constituent Method Date/ID Type Units Cone. QC Data DQO Note Metals Arsenic 6010B 04/06/2004:A 02-CCB mg/L ND <0.01 02-CCV mg/L 1.000 97.7% 90-110 Barium 3050B 03/24/2004:A209 Blank mg/kg ND <0.3 LCS mg/kg 40.00 96.1% 85-115 PDS mg/kg 40.00 103% 75-125 MS mg/kg 40.00 91.1% 75-125 (STK431993-01) MSD mg/kg 40.00 56.7% 75-125 435 MSRPD mg/kg 38.1% 520 435 3010A 04/02/2004:A207 Blank mg/L ND <0.025 LCS mg/L 4.000 98.9% 85.115 PDS mg/L 4.000 104% 75-125 MS mg/L 4.000 97.9% 75-125 (STK431922-01) MSD mg/L 4.000 98.4% 75-125 MSRPD mg/L 0.4% 520.0 STLC 04/08/2004:A217 ExBlk mg/L -0.0035 0.00600 PDS mg/L 0.8000 111% 75-125 ExDup mg/L 2.2% 20 6010B 03/24/2004:A 01-CCB mg/L ND <0.005 01-CCV mg/L 1.000 98.7% 90-110 02-CCB mg/L ND <0.005 02-CCV mg/L 1.000 99.9% 90-110 03/26/2004:A 03-CCB mg/L ND <0.005 03-CCV mg/L 1.000 101% 90-110 04-CCB mg/L ND <0.005 04-CCV mg/L 1.000 102% 90-110 03131/2004:A 03-CCB mg/L ND <0.005 03-CCV mg/L 1.000 103% 90-110 04-CCB mg/L ND <0.005 04-CCV mg/L 1.000 100% 90-110 04/06/2004:A 004CB mg/L ND <0.005 00-ICV mg/L 1.000 99.2% 90-110 01-CCB mg/L ND <0.005 01-CCV mg/L 1.000 97.1% 90-110 02-CCB mg/L ND <0.005 02-CCV mg/L 1.000 97.6% 90-110 04107/2004:A 00-ICB mg/L ND <0.005 00-ICV mg/L 1.000 99.5% 90-110 01-CCB mg/L ND <0.005 01-CCV mg/L 1.000 98.6% 90-110 Beryllium 3050B 03/2412004:A209 Blank mg/kg ND <0.3 LCS mg/kg 40.00 94.5% 85-115 PDS mg/kg 40.00 99.0% 75-125 MS mg/kg 40.00 78.5% 75-125 (STK431993-01) MSD mg/kg 40.00 52.6% 75.125 435 MSRPD mg/kg 39.3% 520 435 Report continued on next page... STK431922: Quality Control Page 2