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April 14, 2004 Lab ID : STK431922 Valley Industries Customer : 3-11146 Quality Control - Inorganic Constituent Method Date/ID Type Units Cone. QC Data DQO Note Metals Molybdenum 6010B 04106/2004:A 00-ICV mg/L 1.000 101% 90-110 01-CCB mg/L ND <0.01 Ol-CCV mg/L 1.000 98.5% 90-110 02-CCB mg/L ND <0.01 02-CCV mg/L 1.000 98.3% 90-110 Nickel 3050B 03124/2004:A209 Blank mg/kg ND <0.5 LCS mg/kg 40.00 94.9% 85-115 PDS mg/kg 40.00 70.0% <li MS mg/kg 40.00 363% <14 (STK431993-01) MSD mg/kg 40.00 177% MSRPD mg/kg 11.3% 520 3010A 04/02/2004:A207 Blank mg/L ND <0.05 LCS mg/L 4.000 102% 85-115 PDS mg/L 4.000 105% 75-125 MS mg/L 4.000 99.4% 75-125 (STK431922-01) MSD mg/L 4.000 100% 75-125 MSRPD mg/L 0.9% 520.0 6010B 03/2412004:A 01-CCB mg/L ND <0.01 01-CCV mg/L 1.000 98.3% 90-110 02-CCB mg/L ND <0.01 02-CCV mg/L 1.000 99.9% 90-110 04/06/2004:A 00-ICB mg/L ND <0.01 00-ICV mg/L 1.000 101% 90-110 01-CCB mg/L ND <0.01 Ol-CCV mg/L 1.000 101% 90-110 02-CCB mg/L ND <0.01 02-CCV mg/L 1.000 100% 90-110 Selenium 3050B 03/2412004:A209 Blank mg/kg ND <0.5 LCS mg/kg 40.00 88.3% 85-115 PDS mg/kg 40.00 98.1% 75-125 MS mg/kg 40.00 77.2% 75-125 (STK431993-01) MSD mg/kg 40.00 51.5% 75-125 435 MSRPD mg/kg 39.4% 520 435 3010A 04/02/2004:A207 Blank mg/L ND <0.05 LCS mg/L 4.000 94.5% 85-115 PDS mg/L 4.000 98.7% 75-125 MS mg/L 4.000 92.6% 75-125 (STK431922-01) MSD mg/L 4.000 94.4% 75-125 MSRPD mg/L 2.0% 520.0 STLC 04/O8/2004:A217 ExBlk mg/L -0.0039 0.0100 PDS mg/L 0.8000 105% 75-125 ExDup mg/L 0.041 0.10 60108 0NW2004:A 01-CCB mg/L ND <0.01 01-CCV mg/L 1.000 100% 90-110 02-CCB mg/L ND <0.01 02-CCV mg/L 1.000 103% 90-110 Report continued on next page... STK431922: Quality Control Page 7