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QC Sample Results <br />Client: Stockton Scavengers Association Inc <br />Project/Site: CA10021Stockton Scavengers <br />------ ------ ..------------ --.... _... _.. <br />Method: 6010B - Metals (ICP) (Continued) <br />Lab Sample ID: 280-41009-2 MS <br />Matrix: Solid <br />Analysis Batch: 15063 <br />TestAmerica Job ID: 280-41009-2 <br />Client Sample ID: METAL SHAVINGS <br />Prep Type: STLC Citrate <br />Lab Sample ID: 280-41009-2 MSD <br />Sample Sample <br />Spike <br />MS MS <br />D %Ree <br />Client Sample ID: METAL SHAVINGS <br />%Rec. <br />Analyte F <br />Result Qualifier <br />Added <br />Result Qualifier <br />Unit <br />D %Rec <br />Limits <br />Thallium <br />ND <br />20.0 <br />18.8 <br />mg/L <br />94 <br />75-125 <br />Vanadium <br />0.88 <br />5.00 <br />5.96 <br />mg/L <br />102 <br />75-125 <br />Zinc <br />24 <br />5.00 <br />29.3 4 <br />mg/L <br />100 <br />75-125 <br />Lab Sample ID: 280-41009-2 MSD <br />LB LB <br />%Rec. <br />Unit <br />D %Ree <br />Client Sample ID: METAL SHAVINGS <br />Matrix: Solid <br />Result Qualifier <br />RL <br />MDL Unit <br />87 <br />D Prepared Analyzed oil Fac <br />Prep Type: STLC Citrate <br />Analysis Batch: 15063 <br />0.20 <br />0.014 mg/L <br />04/26/1315:18 10 <br />Lead <br />ND <br />0.10 <br />Sample Sample <br />Spike <br />MSD MSD <br />Lab Sample ID: LCS 320-1476115-A A10 <br />%Rec. RPD <br />Analyte <br />Result Qualifier <br />Added <br />Result Qualifier <br />Unit <br />D %Ret <br />Limits RPD Limit <br />Silver <br />0.012 J <br />0.500 <br />0.563 <br />mg/L <br />110 <br />75-125 2 20 <br />Arsenic <br />0.15 J <br />20.0 <br />20.2 <br />mg/L <br />100 <br />75-125 1 20 <br />Banum <br />3.9 <br />20.0 <br />23.0 <br />mg/L <br />96 <br />75-125 0 20 <br />Beryllium <br />0.0033 JB <br />0.500 <br />0.476 <br />mg/L <br />94 <br />75-125 0 20 <br />Cadmium <br />ND <br />0.500 <br />0.521 <br />mg/L <br />104 <br />75-125 0 20 <br />Cobalt <br />1.3 <br />5.00 <br />6.22 <br />mg/L <br />99 <br />75-125 0 20 <br />Chromium <br />12 <br />2.00 <br />14.1 4 <br />mg/L <br />106 <br />75-125 0 20 <br />Copper <br />0.24 B <br />2.50 <br />3.06 <br />mg/L <br />113 <br />75-125 1 20 <br />Nickel <br />0.81 <br />5.00 <br />5.18 <br />mg/L <br />87 <br />75-125 0 20 <br />Selenium <br />ND <br />20.0 <br />19.7 <br />mg/L <br />98 <br />75-125 1 20 <br />AnSmony <br />0.22 <br />5.00 <br />4.79 <br />mg/L <br />91 <br />75-125 0 20 <br />Thallium <br />ND <br />20.0 <br />18.8 <br />mg/L <br />94 <br />75-125 0 20 <br />Vanadium <br />0.88 <br />5.00 <br />5.93 <br />mg/L <br />101 <br />75-125 0 20 <br />Zinc <br />24 <br />5.00 <br />29.5 4 <br />mg/L <br />104 <br />75-125 1 20 <br />Lab Sample ID: LB 320-14761/1-A <br />At LB <br />Client <br />Sample ID: Method Blank <br />Matrix: Solid <br />Prep Type: STLC Citrate <br />Analysis Batch: 15206 <br />Lab Sample ID: 280-41009.2 MS <br />Matrix: Solid <br />Analysis Batch: 15206 <br />Analyte <br />Molybdenum <br />Lead <br />Sample Sample Spike MS M8 <br />Result Qualifier Added Result Qualifier <br />- 2.4 10.0 13.0 <br />LID L 5.00 4.33 <br />Client Sample ID: METAL SHAVINGS <br />Prep Type: STLC Citrate <br />LB LB <br />%Rec. <br />Unit <br />D %Ree <br />Limits <br />Analyte <br />Result Qualifier <br />RL <br />MDL Unit <br />87 <br />D Prepared Analyzed oil Fac <br />Molybdenum <br />ND <br />0.20 <br />0.014 mg/L <br />04/26/1315:18 10 <br />Lead <br />ND <br />0.10 <br />0.012 mg/L <br />04/26/1315:18 10 <br />Lab Sample ID: LCS 320-1476115-A A10 <br />Client Sample ID: Lab Control Sample <br />Matrix: Solid <br />Prep Type: STLC Citrate <br />Analysis Batch: 15206 <br />Spike <br />LCS LCS <br />%Rea <br />Analyte <br />Added <br />Result Qualifier <br />Unit <br />D %Ree Limits <br />Molybdenum <br />10.0 <br />10.7 <br />mg/L <br />107 75-125 <br />Lead <br />5.00 <br />4.61 <br />mg/L <br />92 75-125 <br />Lab Sample ID: 280-41009.2 MS <br />Matrix: Solid <br />Analysis Batch: 15206 <br />Analyte <br />Molybdenum <br />Lead <br />Sample Sample Spike MS M8 <br />Result Qualifier Added Result Qualifier <br />- 2.4 10.0 13.0 <br />LID L 5.00 4.33 <br />Client Sample ID: METAL SHAVINGS <br />Prep Type: STLC Citrate <br />TestAmerica Denver <br />Page 13 of 20 5/3/2013 <br />111 <br />l� <br />#sr 5i <br />rti.;,.,...: <br />1 <br />%Rec. <br />Unit <br />D %Ree <br />Limits <br />mg/L <br />106 <br />75-125 <br />mg/L <br />87 <br />75-125 <br />TestAmerica Denver <br />Page 13 of 20 5/3/2013 <br />111 <br />l� <br />#sr 5i <br />rti.;,.,...: <br />1 <br />