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AIR, WATER & HAZARDOUS WASTE LABCOORY (Na.90&131 ) CERTIFIED by COORNIA DEFT of PUBLIC HEALTH <br /> Central Coast <br /> Central Analytical Services, Inc. Lab Number : QS-11119 <br /> Coast 141 Suburban Road, Suite C-4 Collected <br /> Analytical San Luis Obispo, California 93401 Received <br /> Services (805) 543-2553 Tested : 11/11/89 <br /> Collected by: <br /> EXTRACTED BY EPA METHOD 5030 (purge-and-trap) <br /> CCAS EPA METHOD 8240/8260 (GC/MS) <br /> Sample Description: <br /> ROASTED SOIL SPIKE <br /> Spiked with 20 ug/L VOA Stock <br /> Compound Analyzed, Detection Limit Concentration Percent <br /> (ug/L)(POL)* w/spike (ug/L) Recovery <br /> Benzene 0. 1 21 . 110. <br /> Bromodichloromethone 0. 1 22. 110, <br /> Bromoform 0.2 21 . 1041. <br /> Carbon Tetrachloride 0. 1 21 . 100. <br /> Chlorobenzene 0. 1 22. 110. <br /> 2-Chloroethyl Vinyl Ether 1 . not spiked ---- <br /> Chloroform 0.5 21 . 110. <br /> Dibromochloromethone 0. 1 20. 100. <br /> 1 ,2-Dichlorobenzene 0. 1 22. 110. <br /> 1 ,3-Dichlorobenzene 0. 1 23. 120. <br /> 1 ,4-Dichlorobenzene 0. 1 21 . 100. <br /> 1 , 1-Dichloroethane 0. 1 21 . 100. <br /> 1 ,2-Dichloroethane (EDC) 0. 1 20. 100. <br /> 1 , 1-Dichloroethene 0. 1 20. 100. <br /> c-1 ,2-Dichloroethene 0. 1 22. 110. <br /> t-1 ,2-Dichloroethene 0. 1 21 . 110. <br /> 1 ,2-Dichloropropane 0. 1 23. 110. <br /> c--1 ,3-Dichloropropene 0.1 19. 96. <br /> t-1,3-Dichloropropene 0. 1 20. 98, <br /> Ethylbenzene 0. 1 23. 120. <br /> Ethyl Chloride 0. 1 43. 110. <br /> Ethylene Dibromide 0. 1 not spiked ---- <br /> Methyl Bromide 0. 1 42. 110. <br /> Methyl Chloride 0.1 29. 73. <br /> Methylene Chloride 1 . 25. 130. <br /> 1 , 1 ,2,2-Tetrachloroethane 0.5 20. 100. <br /> Tetrachloroethylene (PCE) 0. 1 22. 110. <br /> Toluene 0. 1 21 . 110. <br /> 1 , 1 , 1-Trichloroethane (TCA) 0. 1 21 . 110. <br /> 1 , 1 ,2-Trichloroethane 0. 1 22. 110. <br /> Trichloroethene (TCE) 0. 1 24. 120. <br /> Trichlorotrifluoroethane 0.5 22. 110. <br /> Trichlorofluoromethone 0.5 39. 97. <br /> Vinyl Chloride 0. 1 42. 1910. <br /> Xylenes 0.2 66. 110. <br /> Percent Recoveries of Sample-Specific Quality Assurance Spikes are: 96/100. <br /> MSD#7 <br /> 11-15-89c, ubmi ted, <br /> QS11119v.wr1/132 <br /> MH/tz/jc/kc Mary Havlicek, Ph.D. , President <br />