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3 . 0 AL;Ty AggggANCE PLAN <br /> ral Samplec__ co lock i_on and��flli:��x Proce�3t�re� <br /> Proper collection and handling are essential to erasure the <br /> quality Of a sample. Each sample will be collected in a suitable <br /> container, preserved carr-ctly for the intended analyses, and <br /> sto--d prior to analysis for no longer than the maximum. allowable <br /> holding time. Details on the procedure for collection and han- <br /> aling of soil samples to be used on this project can be found in <br /> Section 1 , 0 (Methods) . <br /> 33 .;._3 ala 1�3ent;f� a zoo a�xd w;�aisA-pf-rgustody Procedures <br /> Sample identification and chain-of-custody procedures ensure <br /> sa-,nV,_e integrity and document sample possession from the time of <br /> collection to its ultimate disposal . Each sample container <br /> submitted analysis will have a label affixed to identify the job <br /> number, date., and time of sample collection, and a sample number <br /> unique to that sample . This information, in addition to a de- <br /> scription of the sample, Field measurements made, sampling <br /> methodology, names of on-sit-e pers=nel , and any other pertinent <br /> field observations will be recorded on the borehole log in the <br /> field records. All samples will be analyzed by a State-certified <br /> laboratory . <br /> A chain-of-custody fort^ will be used to record possession of the <br /> samplo from tine of collection to ifs arrival at the laboratory. <br /> When the samples are shipped, the person in custody of them will <br /> relinquish the samples by signing the chain-of-custody form and <br /> not" the time. The sample-control officer at the laboratory <br /> will verify sample integrity and confirm that it was collected in <br /> the ,roper container, preserved correctly, and that there is and <br /> adequate volume for analysis. <br /> If these conditions are net, the sample will be assigned a unique <br /> log number for identification throughout analysis and reporting. <br /> The log number will be recorded on the chain-of-custody form and <br /> in tie legally-required log book maintained by the laboratory in <br /> the .laboratory. The sample description, date received, client' s <br /> name and any other relevant .information will also be recorded. <br /> ��l�tica], duality. As�UY�S�ca <br /> In addition to routine calibration of the analytical instruments <br /> with standards and blank, the analyst is required to run dupli- <br /> cates and spikes on to percent of the analyses to insure an added <br /> measure of precision and accuracy. Accuracy is also verified <br /> through the following: <br /> 1 . U.S. Environmental. Protection Agency (EPA) and State cer- <br /> tification programs . <br /> Page! 2 <br />