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GeRinalytical Laboratories, It. <br />1405 Kansas Avenue Modesto, CA 95351 Phone (209) 572-M Fax (209) 572-0916 <br />CERTIFICATE OF ANALYSIS <br />Report# K127-07 Oxygenates Date: 5/13/99 <br />Semco Project: 99-5029 (Kahlid Massod) Date Recd: 5/07/99 <br />1217 S 7th Street Date Started: 5/12/99 <br />Modesto CA 95351 ppp Date Completed: 5/12/99 <br />Date Sampled: 5/07/99 <br />Sampler. R Azevedo (Geo) <br />Sample ID <br />Lab ID <br />MDL <br />Method <br />Analyte <br />Results Units <br />TK2-South 0 15' <br />K21623 <br />10 <br />8260 <br />Methyl tertiary -Butyl Ether (MTBE) <br />ND pg/KK <br />10 <br />Ethanol <br />ND <br />100 <br />tertiary -Butanol <br />ND <br />10 <br />Di -isopropyl ether (DIPE) <br />ND <br />10 <br />Ethyl tertiary -Butyl Ether (ETRE) <br />ND <br />10 <br />tertiary -Amyl Methyl Ether (TAME) <br />ND <br />TK2-North 0 15' <br />K21624 <br />10 <br />8260 <br />Methyl tertiary -Butyl Ether (MTBE) <br />740 PX/KK <br />10 <br />Ethanol <br />ND <br />100 <br />tertiary -Butanol <br />2600 <br />10 <br />Di -isopropyl ether (DIPE) <br />ND <br />10 <br />Ethyl tertiary -Butyl Ether (ETRE) <br />ND <br />10 <br />terttary-Amyl Methyl Ether (TAME) <br />ND <br />TKl-South 0 12' <br />K21626 <br />2000 <br />6260 <br />Methyl tertiary -Butyl Ether (MTBE) <br />160000 WKR <br />2000 <br />Ethanol <br />ND <br />20000 <br />tertiary -Butanol <br />ND <br />2000 <br />Di -isopropyl ether (DIPE) <br />ND <br />2000 <br />Ethyl terhary-Butyl Ether (ETBE) <br />ND <br />2000 <br />tertiary -Amyl Methyl Ether (TAME) <br />ND <br />TKI-North 0 12' <br />K21627 <br />500 <br />8260 <br />Methyl tarda y Butyl Ether (MTBE) <br />31000 *Xg <br />500 <br />Ethanol <br />ND <br />5000 <br />tertiary -Butanol <br />ND <br />500 <br />Di -isopropyl ether (DIPE) <br />ND <br />500 <br />Ethyl tertiary -Butyl Ether (ELBE) <br />ND <br />500 <br />tertiary -Amyl Methyl Ether (TAME) <br />ND <br />Dispenser #19 4West <br />K21628 <br />10 <br />8260 <br />Methyl tertiary -Butyl Ether (MTBE) <br />PK/KK <br />10 <br />Ethanol <br />ND <br />100 <br />tertiary -Butanol <br />ND <br />10 <br />Di -isopropyl ether (DIPE) <br />ND <br />10 <br />Ethyl tertiary -Butyl Ether (ETBE) <br />ND <br />10 <br />tertiary -Amyl Methyl Ether (TAME) <br />ND <br />