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12-09-199' 09:04PIl FRGI-1 TI] 19098651,2144 P.00-. <br /> Omfum VERMCATION LABORATORY ANALYSIS <br /> TANK TANK TPH-G TPH-D BTX & E CL HC TOTAL MTBE METALS PCS <br /> /I i CONTENTS 8015 8015 8070 80I0 LEAD TBA.DIPE ICRP/ 8270 <br /> I i 5260 8260 3260 8240 7420 Me.TAME AES or 8080 <br /> 7,121 3020 AA <br /> 8260 <br /> LEADED GAS X X X X <br /> UNL GAS X X X <br /> DIESEL X X <br /> j - <br /> KEROSENE X X <br /> j UNK FUEL X X X X X <br /> PROD. OIL X X -- <br /> CHLOR - <br /> SOLVENTS X X <br /> NONCHLOR <br /> SOLVENTS X X X <br /> WASTE\ <br /> USED OIL X X X X X X <br /> ,dl analysis methods are the designated EPA methods described in EPA SW 846, Third Edition. Those methods not found m <br /> W 346 arc specifically noted below. Refer to the "SWRCB LUFI' Field Manual", Appendix D (B), Table 3-5 on page A20 <br /> br minium detection limits for motor vehicle fuel (gasoline and diesel). Rtfcr to 1-2-3 "Regional Board Staff <br /> ecornmendations for Initial Evaluation and Investigation of UST's" for the waste and motor oil minimum detection limits, <br /> etectiolm Limits that remain below the MCL, MC or Allowable Limit of the contaminant in. question will be accepted, <br /> toweveri laboratory shall utilize the most conservative method. <br /> ABORATORY ANALYSES TERMINOLOGY: <br /> PH-Ci Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 5015 mod or GC/hlS 8260 <br /> PH-D Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GC/MS 8260 <br /> STX & E Benzene. Toluene, Xylene & Ethyl Benzene, GC/PID 807.0 or GC/MS 8260 <br /> �L 14C ; Chlorinated Hydrocarbon, GC/HSD 8010, GC/MS 8240 <br /> OTAL LEAD Total lead, AA 7410, AA 7421 or ICP-AES 6010 <br /> # TBE Methyl Tcruazy Butyl Ether, GC/PID 8020 and confirmed by GC/MS 8260 <br /> ETALS ICRP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7000. Metals: Cadmium, Chromium in and VY, Lead, Zinc and Nickel. <br /> CB ! Polychlorinated Biphenyls, GC/MS 8270 or 8080 <br /> 'C-FID I Gas Chromatography, Flame Ionization Detection <br /> ethod 1050 Acid digestion <br /> ethod 540 SoxWet sample preparation <br /> ethod 550 Sonication sample preparation, extraction method <br /> ethod 30 Purge and trap sample preparation <br /> 4 <br /> A/QC Quality Assurance/Quality Control <br /> i <br /> Notes: T�O avoid false positive detection of benzene, benzene-free solvents are to be used. Fused capillary columns are <br /> referred ito packed columns; a packed column may be used as a "first cut" with "dirty' samples or once the hydrocarbons have <br /> t'icen characterized and proper QA/QC is followed. <br /> or dnnkkug water sources, EPA recommends that the 500 series for volatile organic should be used in preference to the 600 <br /> ,je:ries bec6ose the detection limits:ire lower and the QA/QC is bcttcr. Samples czltibiting any level of heavy metal <br /> conramint itton may require further analysis. PHS-EHD recommends holding those samples until disposal is indicated. <br /> i <br /> ii <br /> H 23 04:6 (Revised 10124197) Page 8 <br /> i <br /> i <br />