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INITIAL CALIBRATION <br /> EPA METHOD 5030/M8015 <br /> INSTRUMENT ID: GC #8 SDG: 95K036 <br /> DATE: 09/30/95 <br /> GASOLINE BROMOFLUOROBENZENE <br /> DATA <br /> FILE CONC. RESPONSE CONC. RESPONSE <br /> ppb AREA FACTOR ppb AREA FACTOR <br /> BJ01-11 100 570186 1.75E-04 20 46502 4.30E-04 <br /> BJ01-12 200 961015 2.08E-04 30 77620 3.86E-04 <br /> BJ01-13 500 2462090 2.03E-04 50 129697 3.86E-04 <br /> BJ01-14 2500 12280258 2.04E-04 80 184654 4.33E-04 <br /> BJ01-15 5000 21446484 2.33E-04 100 248501 4.02E-04 <br /> % Relative Std. Deviation 9% % Relative Std. Deviation 5% <br /> Average Response Factor 2.05E-04 Average Response Factor 4.08E-04 <br /> DAILY CALIBRATION CHECK <br /> DATE DATA FILE DCC# RF % DIFF. % SURR.REC. COMMENTS <br /> 11/21/95 BK20-27 3 1.89 8 105 <br /> 11121195 BK20-41 4 2.01 2 104 <br /> 11121/95 BK20-52 5 1.78 13 104 <br /> 11/21/95 BK20-64 6 2.06 0.5 107 <br /> /1122195 BK20-80 7 1.98 3 119 <br /> STANDARDS <br /> ANALYTE GASOLINE BFB <br /> Int. Standard S 16A-01-01-03 S16C-01-13-02 <br /> Conc. (ppm) 5000 50 <br /> OC LIMIT: IC : RSD < 20% <br /> DCG: D < 15% <br /> 0 <br /> 006 <br />