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• PUBLIC HEALTH SERVI!:E� <br />San Joaquin Co <br />P.O. Box 2009 <br />1C01 East Hazelton Avenue <br />Stoc4;ton, California 95201 <br />M CLOSURE PLAN REVIEW COEMIST MINI n( VLRIFI CATION LAB ANALySES <br />TANK COWM <br />Waste Pro( <br />LEADED GAS( <br />UNL GASC <br />F <br />OKNOWN FUE <br />OIL <br />CHLOR. SOLV <br />NONCHLOR. S <br />WASTE/USED <br />VTS <br />luct <br />)LINE <br />)LINE <br />TPN -C <br />GC -FID <br />(5030) <br />--- <br />1PI1-D <br />CC -FID <br />(5030) <br />-_ _ <br />TEPII <br />(3550) <br />(3540) <br />-- <br />D'11X&E <br />(8020) <br />CL IIC <br />(8010) <br />(8240) <br />ITL <br />(D <br />CDD <br />0 H S) <br />ML'CALS <br />(IC7 - <br />AES) <br />PCB <br />(02'10) <br />(0000) <br />-- <br />x <br />x <br />- <br />- <br />ENTS <br />-- <br />— <br />-- — <br />-- <br />-- <br />-- <br />KTS <br />— <br />-- <br />---- <br />--- - <br />— <br />-- <br />MINIMUM VERIFICATION LABORATORY ANALYSES TERMINOLOGY <br />The following listing of <br />terminology used will be <br />described in EPA SW 8460 <br />s(Mclfically noted. <br />X <br />CTI HC 80100OR) <br />8240 <br />TEC. (DOHS-LUFT) <br />EDB (DOHS -AB 1803) <br />GC FID <br />ICP -AES OR AA <br />Method 5030 <br />Method 3550 <br />Method 3540 <br />QA/QC <br />laboratoryy analyses abbreviations is provided as a guide so tlk�t <br />more familiar. All analyses methods are designated rPA methods as <br />Third Edition. 'Those methods not found In SW 846, are <br />Total Petroleum Ilydrocarbon, Gasoline <br />Total Petroleum Hydrocarbon, Diesel <br />Total Extractable Petroleum Hydrocarbon (8015) <br />Benzene, Toluene, Xylene 6 Ethyl Benzene (8020) <br />Chlorinated Ilydr-(o(carbon 8010 or 8240 <br />Ethyleneydlbranlde0(D0119-A 1003) <br />Gas Chromatography Flame lon47atlon Detector <br />Inductively Coupled Plasma Atomic Emission Spectrometry or Atomic <br />Absorption Spectrometry <br />Purge and Trap Sample Preparation <br />Sonication Sample Preparation <br />Soxhlet Sample Preparation <br />Quality Assurance/Quality Control <br />Notes! To avoid false positive detection of benzene, benzene -free solvents are to be used. <br />Fused capillaryy columns are preferred to packed columns; a packed column may be used as a <br />"first cut" vith "dirty" samples or once the hydrocarbons have been characterized and <br />Proper OA/QC is folloved. <br />organicsFbe usedkIngpreferencertostheP600eseriesdbecausetthe5detection limitslarel]over and <br />the OA/QC is better. <br />SITE ADDRESS .20Yi 70AI JTOCKTUAJ <br />SWEEPS I /d 7 <br />CONTRACTOR— /` APPROVAL DATE (" <br />