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Barry H. Nicholson CERTIFICATE OF ANALYSIS <br /> Port of Stockton Friday,January29, 1999 <br /> 2201 W.Washington St. ,(. D <br /> Stockton GA. 95205 <br /> Sample Information 1 <br /> Sample ID: PE4137-01 Sample Type: Grab 4 <br /> Sample Description: Tank Site#8 Project A'ame: Site#8 ` <br /> Date/Time Sampled: 1/5/99 3:.00:00 PM Sample Matrix: Soils <br /> ANALYTICAL RESULT QA/QC R.EPORT�� <br /> Date LCS Spike MS Spike <br /> Test Parameter Method DLR Unit Result Dilution Analyzed Blank Colic. LCS% Conc. MS% MSD RSD% <br /> Lead (Pb) EPA 6020 1 mg/kg 2.50 19 NO 20 85.5%° 20 90.0% 89.0% 0.3% <br /> Benzene EPA 8260 0.005 mglKg NO 1 ND 10 95.0% 10 95.0% 92.0% 0.8% <br /> Toluene EPA 8260 0.005 mg/Kg NO 1 ND 10 92.0% 10 90.0% 91.0% 0.3%° <br /> Ethylbenzene EPA 8260 0.005 mg/Kg NO 1 ND 10 92.0% 10 96.0% 91.0% 1.3% <br /> Xylenes,Total EPA 8260 0.005 mg/Kg NO 1 NO 10 93.0% 1091.0% 90.0% 0.3% <br /> Methyl-t-Butyl Ether(MtBE) EPA 8260 0.005 mg/Kg NO 1 NO 10 6U% 10 92.0% 94.0% 0.5% <br /> Diisopropyl ether(D1PE) EPA8260 0.005 mg/Kg NO 1 ND 10 11100.0% 10 98.0% 99.0% 0.3% <br /> Ethyl-t-butyl ether(ETBE) EPA8260 0.005 mg/Kg NO 1 ND 10 91.0% 10 94.0% 95.0% 0.3% <br /> Tert-amyl methyl ether(TAME) EPA8260 0.005 mg/Kg NO 1 ND 10 97.0% 10 96.0% 96.0% 0.0% <br /> t-Butanol (TBA) EPA8260 0.05 mg1Kg ND 1 ND 10 90.0% 10 94.0% 95.0% 0.3% <br /> TPFI-Gas EPA8260 0.5 mg/Kg NO 1 NO 1 98.0% 1 99.0% 97.0% 0.5% <br /> r <br /> EPA-Envvronme tal Protection 11gencil Method. Page 1 of 2 <br /> SM-Standard Method for Examination of Water.Wastewater 181h Ed. <br />