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Barry H. Nicholson CERTIFICATE OF ANALYSIS <br /> Port of Stockton lrittay,January 29, 1999 <br /> 2201 W. Washington St. , <br /> (:. D <br /> Stockton CA. 95205 <br /> C [ W <br /> Sample Information <br /> Sample ID: PE4137-02 Sample Type: Grab o rffl <br /> Sample Description: Stockpile Site#8 PYofect Name: Site#8 <br /> Date/Time Santpled: 1115/99 3:05:00 PM Sample Matrix: Soils <br /> ANALYTICAL RESULT . QA/OCREPORT <br /> Date LCS Spike MS Spike <br /> Test Parameter Method DLR Unit Result Dilution Analyzed Blank Colic. LCS% Colic. MS% MSD RSD% <br /> Lead (Pb) EPA 6020 1 mg/kg 11.90 19 ND 20 85.5% 20 90.0% 89.0% 0.3% <br /> Benzene EPA 8260 0.005 mg/Kg ND 1 ND 10 95.0% 10 95.0% 92.0% 0.8% <br /> Toluene EPA 8260 0.005 mg/Kg ND 1 ND 10 92.0% 10 90.0% 91.0% 0.3% <br /> Ethylbenzene EPA 8260 0.005 mg/Kg ND i # ND 10 92.0% 10 96.0% 91.0% 1.3% <br /> Xylenes,Total EPA 8260 0.005 mg/Kg ND 1 f ND 10 93.0% 10 91.0% 90.0% 0.3% <br /> x_ <br /> Methyl-t-Butyl Ether(MISE) EPA 8260 0.005 mg/Kg ND 1 TT ND 10 99.0% 10 92.0% 94.0% 0.5% <br /> Diisopropyl ether(DIPE) EPA8260 0.005 mg/Kg ' ND 1 ND 10 100.0% 1D 98.0% 99.0% 0.3% <br /> Ethyl-t-butyl ether(ETRE) EPA8260 0.005 mg/Kg ND 1 ND 10 91.0% 10 94.0% 95.0% 0.3% <br /> Tert-amyl methyl ether(TAME) EPA8260 0.005 mg/Kg ND 1 ND 10 97.0% 10 96.0% 96.0% 0.0% <br /> t-Butanol (TBA) EPA8260 0.05 mg/Kg ND 1 ND 10 90.0% 10 94.0% 95.0% 0.3% <br /> TPH-Gas EPA8260 0.5 mg/Kg ND 1 ND 1 98.0% 1 99.0% 97.0% 0.5% <br /> 3 <br /> s• <br /> L <br /> i <br /> EPA-Environmental Protection Agency Method. Page I of 2 <br /> SM-Standard hfethod for Examination of Wafer ffasteivaler I Sfh Ed. <br />