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/18/2005 09:01 20903 EHD PAGE 06 <br /> r MINIMUM VERIFICATION IABORATORYANALYSIS <br /> TANK TANK TPH•GTPH•D BTX do E CL HC TOTAL MTBE AS EN kL AI, <br /> s CONTENTS 8015 8015 <br /> 8260 8020 8010 LEAD 8020 (MTBE, PCB <br /> 8260 8260 8240 7420 8260 TSA,DD�E, .ICAP/ 8270 <br /> 8260 1421 ETBB, AES w 8080 <br /> TAME) AA <br /> 3260 <br /> X X <br /> UNL GX X <br /> X X <br /> X <br /> X X <br /> KEROSENE X X <br /> X <br /> LINK FUEL X X X <br /> X X <br /> PROD.OIL X X <br /> X <br /> CHLOR. <br /> SOLVENTS X X X <br /> NONCHLOR <br /> SOLVEN're X X X <br /> WASTE\ <br /> USED OIL X X X <br /> X <br /> All analysis methods arc the desigrmted EPA methods descrlbed In EPA SW 846,Third Edition. TbO3e methods not found X SW $46 are <br /> specifically noted below, Refer to the "SWhCB LUF')'Field Manual",Appendix D (B),limits for motor vehicle fuel (gesallnt and diesel). Refer to " I ) Table 3.5 on page A20 for minimum detection <br /> lnvesGsellon o(US's' for the waste and motor oil minimum detection limits. Deteetloa Limits that roard SIGIT temainsbelow the MCL,for lnitjj t$TLC or <br /> Allowable Limit or the contamlmant in question will be accepted,however laboratory$ball utilize the most ccnservattvc method. <br /> TPH-G Total Penoleum Hydrocahmt,Gasolinq GGFIDLABOIL(030)i015 mod TORY SESor TE NOLOGY; <br /> 1PH.D Total Petroleum Hydrocar11260 <br /> bon,Diesel,GC/FID(3550),8013 mod or GC/MS 8260 <br /> "X 6E\ EBc eae,Toluenc,Xylcne&Edryl Ben2cne,GGPID 8020 or GC/MS 8260 <br /> CL HC Chloriomcd llydrocution,GGHSD 8010,GC/MS M$ 2 Of G <br /> TOTAL LEAD 1'oml IeaQ AA 7420, AA 7421 or ICP-AES 6010 <br /> OXYGENATES MIBE,ETBL,TAME,DIPE,&TBA <br /> METALS ICA?w AA GGMS 8260(For MTBE Wyly you may use 8020) <br /> Inductively Coupled Phumo Atomic Emisdon Spectrometry 6010 or Atomic Absorption Spectrometry 7000, Mctals: <br /> PCB <br /> Cadmium,Chromium III and VI,Lead,zine and Nickel. <br /> Polychlorinucd Biphonytt,GC/MS 8270 or 8080 <br /> GC•FID Gu Chromajography,flame Ionization DetectionMethod 7050 Acid digestion <br /> Mctbod 3540 Soxhlcl sample preparation <br /> Medved 3550 S0nIeelUon sample prepvui0a,extraction method <br /> Method 5030 Purse tad trap sample preparation ' <br /> QA/QC Quality Aasurnnce/Quallry Control <br /> Notes' To awid(al$c positive detection of benzene,ben2cnc-tree solvents are to be used. Fused eapillaly column,aro Prafcrred to vueked wlumns;a <br /> packed column may be used xs a"fico cut"w,rh"dirty"sample$or once the hydroearbona have beam eharaetenzed endProper A/Q <br /> ar^1w8 water i/x11Ce5�EPA rcwmn$rutds thu the 500 aeries for volatile Organic should be used in <br /> tim�u ere lower and the A/ Q Cis followed. For <br /> Q QC Is better. Samples cXhilsAins any level of heavy metal contaminationeay requite further analysiswies ?PHS ERD�ctmn <br /> reconunends holding those samples until disposal is indicated. <br /> EH 23 046 (Revised 05/09100) <br /> 5 <br />