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Soil samples for volatile, scnvvolatile arad nonvolatile analyses are all Collected in prep erly <br /> prepared new brass liners which are 2 inches in diamoter'by A inches in length. Closure is <br /> accomplished with press fit plastic end caps wtaich are ft-ted to tho open ends of brass tube <br /> liners after a sheet of aluminum foil is wrapped over the exposed sample material. No <br /> preservative other than cold storage is used er, samples captured in sample containers of <br /> This type. <br /> Sample handling Procedures <br /> Solid sample material is captured by advancing the liner into the soil. This may be done <br /> by pushing the liner into soft soils or by Containing the, liner in a drive shoe which can be <br /> advanced and then retracted by means of a slide hamtner. Th-,open ends of the sample <br /> liner are covered with aluminum foil and plastic end caps. Tire brass liner is labeled wilt <br /> the appropriate identification numbers which specify the sampling activity designation <br /> number, sample collection area, depth etc, that apply to d0A particular sample. The sample <br /> Liner is then placed in an ice chest which contains pre-frozen blocks of an inert ice substi- <br /> tute such as Blue Ice or Super Ice. <br /> Water samples are collected in any of several appropriate devices such as bailers, Coliwa- <br /> sas, Middleburg sampling pumps, etc., which s_-c described in detail only as warramed by <br /> their employment at a given site. Sample liquid is decant:d into new sample containers in <br /> a manner which reduces the loss of volatile coastitucttr-,and follows the applicable HPA <br /> procedures for handling volatile organic and,,m -volarle compounds. Orly two varia- <br /> tions from the EPA methods axe gene.-ally employed First, preservative is added to the <br /> sample container pror to addition of the sam-- liquid. This method was pioneerrd by <br /> Stoner Laboratories in 1982 and subsequently adopted by laboratories and environmental <br /> consulting funis as a practical m=ans of reducing Ot time that a liquid is allowed to aerate <br /> prior to closure of the sampling container. Second, becaust,, tests have shown that the <br /> preservative readily mixes with sample liquid, glass stirring rrK's arc trot used to agitate the <br /> sample/preservative mixture. <br /> Sample Designations <br /> Al sample containers are identified wit![ botF 2 s mpling event number and a discrete <br /> sample identification nutnbtr. the sarrplirg zvc^t nunibe is the number that appears on <br /> our chain of custody. It is roughly equivaleat to a job number, but applies only to work <br /> done on a particular day of the year, ra-lie. than. ;p<nulr:g several days m jobs and projects <br /> often do. This is followed by the sample I,D. tai:nber which is use lly a simptc number <br /> such as#1, #2, #3. <br /> Chain of Custody <br /> Samples are eontiruously rnainttined in eirhx a :_hilted ice chest, refrigerator. or fieezer <br /> from the time of eollcetivr until aa_cp! r c e S[a[e cc^ifi: d 1la2,ardous Malcr:als <br /> Testing Laboratory, cle:t:d to p`iionii t 1 _311 p r h dJre�, if til;: s.: nples , taken <br /> charge of by a diffemnt party (such as cn b 1 -surf front oar of!,---, a counc , etc.) prior <br />