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• 1455 McDowell Blvd,North Ste D <br /> Sequoia Petaluma, 79 94954 <br /> (707)792-1865 <br /> Analytical FAX(707)792-0342 <br /> www.sequoialabs.com <br /> MACTEC E&C-Petaluma Project:General Commercial P412379 <br /> 5341 Old Redwood Highway,Suite 300 Project Number:Sears/Tracy-UST/AST-3205040383.02 Reported: <br /> Petaluma CA,94954 Project Manager:Gary Lieberman 01/05/05 10:53 <br /> Semivolatile Organic Compounds by EPA Method 8270C-Quality Control <br /> Sequoia Analytical-Petaluma <br /> Repotting Spike Source %RBC RPD <br /> Analyte Result limit Units Level Result %REC Limits RPD Limit Notes <br /> 1 Batch 4120473-EPA 3545 ASE/EPA 8270C <br /> Blank(4120473-BLKI) Prepared: l2/22/04 Analyzed: 12128/04 <br /> 2,4-Dinitrotoluene ND 330 ug/kg <br /> 2,6-Dinitrotoluene ND 330 <br /> Di-noctyl phthalate ND 330 <br /> Fluoranthene ND 330 <br /> Flumen ND 330 <br /> Hexachlorobeazene ND 330 <br /> Hexachlowbutadiene ND 330 <br /> Hexachlorocyclopentadiene ND 330 " <br /> Hexachloroethane ND 330 <br /> Indeno(1,2,3-cd)pyrene ND 330 <br /> Isophorone ND 330 ' <br /> 2-Methyl aphthalene ND 330 „ <br /> 2-Methylphenol ND 330 <br /> 4-Methylphenol ND 330 <br /> Naphthalene ND 330 " <br /> 2-Nitroaailine ND 1700 „ <br /> 3-Nitroaniline ND 1700 <br /> 4-Nitroani(ine ND 1700 <br /> Nitrobenzene ND 330 <br /> 2-Nitrophenol ND 330 <br /> 4-Nitrophenol ND 1700 <br /> N-Nitrosodimethylamine ND 330 " <br /> LN-Nitrosodiphenylamine ND 330 <br /> N-Nitrosodi-n-propylaminc ND 330 <br /> Pentachlorophenol ND 1700 " <br /> Phenanthrene ND 330 ; <br /> Phenol ND 330 <br /> Pyrene ND 330 <br /> 1,2,4-Trichlorober zene ND 330 " <br /> 2,4,5-Trichlorophenol ND 330 ; <br /> 2,4,6-Trichlorophmol ND 330 <br /> Surrogate.,1-Fluorophenol 2010 5000 40 30-101 <br /> ' Surrogate:Phenol-d6 2520 5000 50 33-110 <br /> Surrogate:Nitrobenzene-d5 1890 3330 57 38-117 <br /> Surrogate:2-Fluorobiphenyl 1950 3330 59 48-117 <br /> Sequoia Analytical-Petaluma The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.Unless otherwise staled,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 42 of 46 <br />