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CLIENT: ICrazan&Associates,Inc. ANALYTICAL QC SUMMARY REPORT <br /> Work Order: 0307083 <br /> TestCode: 8260S <br /> Project: <br /> Sample ID BLANKAD SampType: MBLK TestCode: 8260_S Units: pg/Kg Prep Date: 712812003 Run ID: VOCGCMSI_030728A <br /> Client ID: 72277 Batch ID: R1803 TestNo: SW8260B Analysis Date: 7/28/2003 SegNo: 29688 <br /> Analyte Result PCL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> Benzene ND 10 <br /> Ethyl tert-butyl ether(ETBE) ND 10 <br /> Ethylbenzene ND 10 <br /> Isopropyl ether(IPE) ND 10 • <br /> Methyl tert-butyl ether(MTBE) ND 10 <br /> t-Butyl alcohol(t-Butanol) ND 50 <br /> tert-Amyl methyl ether(TAME) ND 10 <br /> Toluene ND 10 <br /> Xylenes,Total ND 10 <br /> SUM 4-Bromofluorobenzene 26.55 0 35.72 0 74.3 65 135 0 0 <br /> Surr:Dibromofluoromethane 24.73 0 35.72 0 69.2 65 135 0 0 <br /> Sample ID Blank-1D SampType: MBLK TestCode: 8260_S Units: pg/Kg Prep Date: 712912003 Run ID: VOCGCMSt_030729A <br /> Client ID: 77772 Batch ID: R1804 TestNo: SW8260B Analysis Date: 712912003 SegNo: 29704 <br /> Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> Benzene ND 10 <br /> Ethyl tert-butyl ether(ETBE) ND 10 <br /> Ethylbenzene ND 10 <br /> Isopropyl ether(IPE) ND 10 • <br /> Methyl tert-butyl ether(MTBE) ND 10 <br /> t-Butyl alcohol(t-Butanol) ND 50 <br /> tert-Amyl methyl ether(TAME) ND 10 <br /> Toluene ND 10 <br /> Xylenes,Total ND 10 <br /> Surr:4-Bromofluorobenzene 25.82 0 35.72 0 72.3 65 135 0 0 <br /> Surr: Dibromofluoromethane 24.35 0 35.72 0 68.2 65 135 0 0 <br /> Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits B-Analyte detected in the associated Method Blank <br /> 1-Analyte detected below quantitation limits R-RPD outside accepted recovery limits Page 2 of 5 <br />