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Date: 31-Jul-03 <br /> Torrent Laboratory, Inc. <br /> CLIENT: Krazan&Associates,Inc. ANALYTICAL QC SUMMARY REPORT <br /> Work Order: 0307087 TestCode: 601OB_S <br /> Project: <br /> Sample ID M8-421 SampType: MBLK TestCode: 6010B_S Units: mg/Kg <br /> Prep Date: 7/2912003 Run ID: ICP_030730C <br /> Client ID: 77777 <br /> Batch ID: 421 TestNo: SW60l0B (SW3050B) Analysis Date: 713012003 SegNo: 29883 <br /> Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> Lead ND 0.35 <br /> EAnalyte <br /> CS-021 SampType: LCS TestCode: 60108_S Units: mg/Kg <br /> Prep Date: 712912003 Run ID: ICP_030730C • <br /> ]777 <br /> Batch ID: 421 TestNo: SW6010B (SW3050B) Analysis Date: 713012003 SegNo: 29881 <br /> Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val °/RPD RPDLimit Qual <br /> Lead 99.65 0.37 100 0 99.6 80 120 0 <br /> 0 <br /> Prep Date: 712912003 Run ID: ICP_030730C <br /> EAnalyte <br /> CSD-421 SampType: LCSD TestCode: 6010B_S Units: mg/Kg SegNo: 29882 <br /> 7777 <br /> Balch ID: 421 TestNo: SW6010B (SW3050B) Analysis Date: 7/3012003 <br /> Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> Lead 98.12 0.37 100 0 98.1 80 120 99.65 1.54 20 <br /> • <br /> B-Mal detected n the associated Method Blank <br /> Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits Y� <br /> 7-Analyte detected below quantitation limits <br /> R-RPD outside accepted recovery limits Page 1 Of 4 <br />