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TORRENT LABORATORY, INC. <br /> 483 Sinclair Frontage Rd. • Milpitas, CA 95035 • Ph: (408) 263-5256 • Fax:(408) 263-8293 <br /> ! Visit us at www.torrentlab.com email:analysis@torrentlab.com <br /> Certified Analytical Report of <br /> Pur¢eable Volatile Organics <br /> Report prepared for: AR Morrill <br /> Date Received: 725/2003 <br /> ! Kra=&Associates,Inc. — Date Reported: 7/302003 — <br /> Client Sample ID: SPB-3 Lab Sample ID: 0307083-005A <br /> Sample Location: PG&E Facility,Tracy <br /> Date Prepared: 7282003 <br /> Sample Matrix: PEAGRAVEL <br /> Date/Time Sampled 7/25/2003 <br /> Parameters Analysis Date Dilution MRL Result — Units <br /> Method Analyzed Factor <br /> Benzene _- � -- _- SW8260B 7/28/2003 10 1 10 ND p9/K9 <br /> Ethyl tert-butyl ether(ETBE) SW8260B 7/28/2003 10 1 10 ND pg/Kg <br /> Ethylbenzene SW8260B 7/28/2003 10 1 10 ND p9/K9 <br /> Isopropyl ether(IPE) SW8260B 7/28/2003 10 1 10 ND pg/Kg <br /> Methyl tert-butyl ether(MTBE) SW8260B 7/2812003 10 1 10 ND pg/Kg <br /> t-Butyl alcohol(t-Butanol) SW8260B 7/2812003 50 1 50 ND pg/Kg <br /> tert-Amyl methyl ether(TAME) SW8260B 7/28/2003 10 1 10 ND pg/Kg <br /> Toluene SW8260B 7/28/2003 10 1 10 ND pg/K9 <br /> SW8260B 7/2812003 10 1 10 ND pg/Kg <br /> Xylenes,Total <br /> 7/2812003 0 1 65 <br /> Surr:4-Bromofluorobenzene SW8260B -135 84.3 %REC <br /> Sur:Dibromofluoromethane SW8260B 7128/2003 0 <br /> 1 65-135 80.5 °hREC <br /> t <br /> These analyses were performed according to State of California Environmental Laboratory Page 14 of 49 <br /> Accreditation program,Certificate#1991 <br />