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• <br /> xe = measured value for spiked sample, <br /> xu = measured value for unspiked sample, and <br /> K = known value of the spike in the sample. <br /> Using the following equation yields the percent recovery <br /> (%R) • <br /> %R = 100 (x, - x,)/ K <br /> BLANK: see Equipment Rinsate, Method Blank, Trip Blank. <br /> CONTROL SAMPLE: A QC sample introduced into a process to monitor the <br /> performance of the system. <br /> DATA QUALITY A statement of the overall level of uncertainty that a <br /> OBJECTIVES (DQOs) : decision-maker is willing to accept in results derived <br /> from environmental data (see reference 2, EPA/QAMS, July <br /> 16, 1986) . This is qualitatively distinct from quality <br /> measurements such as precision, bias, and detection limit. <br /> DATA VALIDATION: The process of evaluating the available data against the <br /> project DQOs to make sure that the objectives are met. <br /> Data validation may be very rigorous, or cursory, <br /> depending on project DQOs. The available data reviewed <br /> will include analytical results, field QC data and lab QC <br /> data, and may also include field records. <br /> DUPLICATE: see Matrix Duplicate, Field Duplicate, Matrix Spike <br /> Duplicate. <br /> EQUIPMENT BLANK: see Equipment Rinsate. <br /> EQUIPMENT RINSATE: A sample of analyte-free media which has been used to <br /> rinse the sampling equipment. It is collected after <br /> completion of decontamination and prior to sampling. This <br /> blank is useful in documenting adequate decontamination of <br /> sampling equipment. <br /> ESTIMATED The lowest concentration that can be reliably achieved <br /> QUANTITATION within specified limits of precision and accuracy during <br /> LIMIT (EQL) : routine laboratory operating conditions. The EQL is <br /> generally 5 to 10 times the MDL. However, it may be <br /> nominally chosen within these guidelines to simplify data <br /> reporting. For many analytes the EQL analyte <br /> concentration is selected as the lowest non-zero standard <br /> in the calibration curve. Sample EQLs are highly matrix- <br /> dependent. The EQLs in SW-846 are provided for guidance <br /> and may not always be achievable. <br /> ONE - 24 Revision 1 <br /> July 1992 <br />