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GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr. Turlock,CA 95380 Phone(209)669-0100 Fax(209)668-8516 <br /> email: I o b.geoCatt.net <br /> Report# XIF0123 Project: City of Lodi Date: 06/14/11 <br /> Jim Thorpe, Inc. Date Recd: 06/01/11 <br /> P.O Box 357 <br /> Lodi, CA 95241 <br /> Volatile Organic Chemistry- Quality Control <br /> GeoAnalytical Laboratories, Inc. <br /> Reporting Spike Source %REC RPD <br /> lAnalyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch X001355-EPA 5030 Prepared&Analyzed: 06/01/11 <br /> Blank(X001355-BLK1) <br /> Gasoline ND 1.0 mg/kg <br /> Surrogate: 1,2-Dichloroethane-d4 0.0152 0.02000 76 72-132 <br /> Surrogate:2-Bromo-l-Chloropropane 0.0166 0.02000 83 71-134 <br /> Surrogate:4-Bromofluoroben:ene 0.0178 0.02000 89 74-132 <br /> LCS(X001355-BSI) <br /> Gasoline 1.3 1.0 mg/kg 1.500 87 80-120 <br /> Surrogate: 1,2-Dichloroethane-d4 0.0166 0.02000 83 72-132 <br /> Surrogate:2-Bromo-l-Chloropropane 0.0184 0.02000 91 71-134 <br /> Surrogate:4-Bromofluoroben:ene 0.0187 0.02000 94 74-132 <br /> Matrix Spike(X001355-MS1) Source:XIE2412-05 <br /> Gasoline 1.3 1.0 mg/kg 1.500 ND 86 63-143 <br /> _._.. .- - - ---- --- - -- ----- - --- -- ------ --...----------- ---------- <br /> Surrogate: 1,2-Dichloroelhane-d4 <br /> --Surrogate: l,2-Dichloroethane-d4 0.0165 0.01000 83 72-132 <br /> Surrogate:2-Bromo-l-Chloropropane 0.0176 0.02000 88 71-134 <br /> Surrogate:4-Bromofluoroben:ene 0.0187 0.02000 94 74-132 <br /> Batch X001356- EPA 5030 Prepared&Analyzed:06/01/11 <br /> Blank(X001356-BLKI) <br /> 1,2-Dichloroethane ND 5.0 ug/kg <br /> Di-isopropyl Ether(DIPE) ND 10.0 " <br /> Ethanol ND 400 " <br /> Ethyl tert-Butyl Ether(ETRE) ND 10.0 " <br /> Ethylene dibromide ND 10.0 <br /> Methyl cert-Butyl Ether(MTBE) ND 10.0 " <br /> Tert-Amyl Methyl Ether(TAME) ND 10.0 " <br /> tert-Butanol(TBA) ND 200 " <br /> Surrogate: l,2-Drchloroethane-d4 15.2 20.00 76 66-133 <br /> Surrogate:2-Bromo-l-Chloropropane 16.6 20.00 83 63-139 <br /> Surrogate:4-Bromofluoroben:ene 17.8 20.00 89 64-136 <br /> Certification#2585 <br />