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FRIEDMAN&BRUYA,- INC. <br /> 1�NVIRONMENTAL CHEMISTS <br /> Date of Report: 03/12/04 <br /> Date Received: 02/297/04 <br /> Project: Chevron Historical Pipeline Portfolio -Pompo Property, F&BI 402259 <br /> QUALITY ASSURANCE RESULTS FOR THE ANALYSIS OF WATER <br /> SAMPLES FOR PNA'S BY EPA METHOD 82700 81-NI <br /> laboratory Code. 402200-04 (Matrix Spike) <br /> Percent Percent <br /> Rcporting Spike Sample Recovery Recovery Acceptance RPD <br /> Analvte Units T'evel Res:ult MS MSD Criteria (Limit,20) <br /> Naphthalene n/l,(pph) 5 <0.1 79 85 50-150 8 <br /> Acenaphthylene pg,'L(ppb) 5 <0.1 82 88 50-150 7 <br /> ,kcenaphthene lig/l,(ppb) .5 <0.1 80 86 50-150 7 <br /> Fluorene pg/L(ppb) .5 <0.1 83 89 60-150 7 <br /> Phenanthrene tLg/T, (ppb) 6 <0.1 74 81 50.150 9 <br /> .Anthracene µg./L (ppb) 15 <0:1 68 75 50-150 11 <br /> Fluaranl,hene ',g/L(1)pb) 5 ---0J 72 81 50-150 12 <br /> Pyrene ELg/L(Ppb) 15 <0.1 75 84 50.160 11 <br /> Benz(a)anthracene pg)L(ppb) 5 <0.1 74 85 50.150 14 <br /> Chrysene pg/11(ppb) 5 <0.1 71 81 50-150 12 <br /> Benzo(b)fluoranthene pg/L (ppb) 5 <0,.1 78 90 .50-150 14 <br /> Benzo(k)fluoranthttne n/L(pph) 5 <0.1 76 87 50-1.50 14 <br /> Benzo(a)pyrene µWl-(pleb) 5 --O,l 77 89 50-150 15 <br /> Indeno(I.2..3-eftyrene 1'tg/l,01* 15 <0.1 62 70 50-150 113 <br /> Dibenzo(a,h)anthraeane pg/l,(ppb) 5 <0,1 67 76 50-150 13 <br /> 13enzo(,-_h1J)perylene gg/L(ppb) 5 <0.1 57 68 a0-150 10 <br /> Laboratory Code. 1,aburatory Control Sample <br /> Percent Percent <br /> Reporting Spike Reeovm Recovery Acceptance RPD <br /> Analvte un-Its Level WS LCSD Criteria <br /> (Limit 20) <br /> Naphthalene µtWT, (ppb) 5 95 102 70-107 8 <br /> Acenaphthylene µ1-/T,(ppb) .5 100 108 65-116 8 <br /> Acenaphthene .LL-IT,(ppb) 5 99 108 70-114 9 <br /> Fluorene Pgll,(ppb) 5 96 105 65-113 8 <br /> Phenanthrene pw'T;(ppb) .5 96 102 72-108 6 <br /> Anthracene µg/T,(ppb) 5 94 99 60-106 6 <br /> Fluoranthene ELg/L(ppb) 5 98 103 69-109 5 <br /> Pyrene µgd- (ppb) 5 102 109 75-109 7 <br /> Benz(a)anthracene ug/L(pph) 5 99 105 52-120 6 <br /> Chn sene gfWL ;pph) 5 95 102 61-110 <br /> Benzo(b)fluuranthene 107 115 49-146 7 <br /> Benzo(k')fluoranthent- (t)1)0 104 ill 71-114 7 <br /> Berizo(a)pyrene pg/l,(ppb) 5 1015 112 58-126 6 <br /> lndcno(1,2,3-crl)p3,rcnc ugl,(ppb) 51 85 90 71.108 5 <br /> Dibenzo(a,h)a-ithrucena (ppb) 15 89 015 67-120 6 <br /> Ben zo(g,h,i)pervIcne �-4/L(ppb) 1 -1,06 5 <br /> 79 84 7 <br />