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- gx <br /> AIN <br /> a, <br /> pi IBM VM <br /> AIR, WATER and HAZARDOUS WASTE LABORATORY CERTIFIED by CALIFORNIA DEPT of HEALTH SERVICES <br /> Coast-to-Const Lab Number: QS05061 <br /> Coast-to- Collected: <br /> Coast Analytical Servsuito C�4• Received: <br /> Analytical 141 Suburban flood , g5/06og1 <br /> Services San Luis Qbiapo, California 93401 Collected by: <br /> (805) 543-2953 <br /> FUEL FINGERPRINT ANALYSIS <br /> CAL DHS (TPN Draft)byPA Method 5030Method(pur9e-and/trap)"«C/MS) <br /> Extracted by <br /> SAMPLE DESCRIPTION: <br /> CCAS-NAPA DI Water spiked to 1.42ppm with <br /> Super Unleaded Gasoline <br /> OPAL Expected Actual Percent <br /> Compound Analyzed ug/1 in u9/1 in ug/1 Recovery <br /> 0.045 e7,%Benzene 0.001 0.052 0.74 8896 <br /> 029 <br /> Toluene 0.001 0.02 0.026 909E <br /> Ethylbenzene 0.001 0 0,73 76% <br /> _ 0.001 0.17 __-- <br /> Xylenes0 001 not spiked ----_ <br /> 1,2-Dichloroethane (EDC) ----- ---- <br /> Ethylene Dibromitle (EDB) <br /> 0,001 not spiked <br /> 'total Purgeable Petroleum Hydrocarbons 1.42 1.40 99% <br /> (Gasoline) 0.1 <br /> (Diesel #2, Stoddard Solvent, --^- <br /> Kerosene, Jet Fuel, Mineral Spirits) not spiked <br /> 23% n/a <br /> BTX as a Percent of Total Fuel <br /> -- 79/91/127 <br /> Percent Surrogate Recoveries <br /> •.....w...r....................... <br /> w..r.r.w...• ..r...rr a....r.r.r.....a <br /> *Practical Quantitation Limit <br /> *-Soils sonicated during extraction <br /> would v <br /> Constituents reported sractifoual quontitationlimit� reported if present <br /> at or above the li P c <br /> Respectfully submitted. <br /> C S -to-COA T ANALYTICAL SERVICES <br /> Mary 4licek, Ph.D. <br /> — President <br /> MSD #1-5/7 <br /> OS5061GW.wr1/FFP72 <br /> MH/hc/gbl9b <br /> 3 - <br />