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04/09/2012 04:06 #6212 P-010/016 <br /> 1534 Willow Pass.-„ad,Pittsburg,CA 94565-1701 <br /> McCampbell Analytical Inc g <br /> = �*� Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 <br /> "When Quality Counts" httpJ/www.mccampbe0.com/E-mail:main@mccampbell.com <br /> Ponder Environmental Services Client Project ID: #12-9007;Stolen Date Sampled: 03/10/12 <br /> P.O.Box 1427 Water Date Received: 03/12/12 <br /> Client Contact: John Cupp Date Extracted: 03/13/12 <br /> Benicia,CA 94510 Client P.O.:#728428 Date Analyzed: 03/13/12 <br /> Volatile Organics by P&T and GC/MS(Basic Target List)* <br /> Extraction Method: SW5030B Analytical Method: SW8260B Work Order: 1203319 <br /> Lab ID 1203319-001C <br /> Client ID Fi <br /> Matrix Water <br /> Compound Concentration* DF Reporting # Rcpurl ng <br /> t;m, Compound Concentration DF <br /> Acetone ND<500 50 10 tert-Am l methyl ether TAME ND<25 50 0.5 <br /> Benzene 51 50 0.5 Bromobenzene ND<25 I 50 1 .5 <br /> Bromochloromethane I ND<25 50 0.5 Bromodichloromethane ND<25 { 50 0.5 <br /> Bromaform ND<25 50 0.5 Bromomethane ND<25 50 I 0.5 <br /> 2-Butanone MEK ND<100 50 2.0 t-But 1 alcohol TBA ND<100 50 { 2.0 <br /> n-But I benzene ND<25 { 50-J 0.5 sec-Butyl benzene I ND<25 I 50 10 5 <br /> tert-Butyl benzene ND<25 50 0.5 Carbon Disulfide <br /> _ I ND<25 I 50 I 0.5 <br /> CarboitTetrachloride ND<25 50 0.5 Chlorobenzene ND<25 50 0.5 <br /> Ch(oroethane ND<25 50 0-5 Chloroform ND<25 50 0.5 <br /> Chloromethane ND<25 50 0.5 2-Chlorotoluene ND<25 50 0.5 <br /> 4-Chlorotoluene ND<25 50 0.5 Dibromochloromethane ND<25 0.5 <br /> 1 2-Dibromo-3-chloro ro ane ND<25 50 0.2 1 2-Dibromoethane EDB ND<25 30 0.5 <br /> Dibromomethane ND<25 50 0.5 12-Dichlorobenzene ND<25 50 0.5 <br /> 1.3-DichlorobenzeneND<25 50 0.5 1,4-Dichlorobenzene ND<25 50 0.5 <br /> Dichlorodifluoromethane ND<25 50 0.5 i 1-Dichlomethane ND<25 50 0.5 <br /> 12-_Dichloroethane(1,2-DCA) { ND<25 I 50 { 0.5 11-Dichloroethene { ND<25 I 50 I 05 <br /> \, cis-1,2-Dichloroethene { ND<25 50 I 0.5 trans-1 2-Dichloroethene ND<25 { 50 03 <br /> 1 2-Dichloro ro ane ND<25 50 0.5 13-Dichloro ro ane ND<25 50 0S <br /> 22-Dichloro ro ane ND<25 50 05 1 1-Dichloro ro ene ND<25 50 0.5 <br /> cis-1 3-Dichforo ro ene ND<25 50 0.5 trans-1 3-D ichloroprop en ND<25 50 0.5 <br /> Diiso ra vl ether DIPE ND<25 50 0.5 Eth lbenzene 170 50 OS <br /> Ethyl tert-but 1 ether ETBE ND<25 50 0.5 Freon 113 ND-c500 50 10 <br /> Hexachlorobutadiene ND<25 50 0.5 Hexachloroethane ND<25 50 0.5 <br /> 2-Hexanone ND<25 50 0.5 Iso ro lbenzene ND<25 50 0.5 <br /> 4-I50ro I toluene ND<25 50 0.5 Meth 1-t-but l ether MTBE ND<25 50 0.5 <br /> Methylene chlorid ND<25 50 0.5 4-Meth 1-2- entanone MIBK ND<25 50 0.5 <br /> Naphthalene 35 50 0.5 n-Propyl benzene 28 50 0.5 <br /> Styrene I ND<25 I 50 { 0.5 1,1,1,2-Tetrachloroethane I ND<25 <br /> 50 I 0.5 <br /> 1,1,2,2-Tetrachloroethane ND<25 50 0.5 Tetrachloroethene ND 25 50 0.5 <br /> Toluene 590 50 0.5 12 -Trich(orobenzene ND<25 { 50 0.5 <br /> 1.2 4-Trichlorobenzene ND<25 50 0.5 1 1 1-Trichloroethane ND<25 50 0.5 <br /> 1,1,2-Trichloroethane ND<25 50 0.5 {Trichloroethene I ND<25 I 50 { 0.5 <br /> Trichlorofluoromethane ND<25 50 0.5 12,3-Trichloro ro ane I ND<25 50 OS <br /> 12 4-Trimeth (benzene 260 50 0.5 13 -Trimeth (benzene 69 50 { 0.5 <br /> Vinyl Chloride ND<25 50 0.5 Xylenes,Total 1000 50 0.5 <br /> Surrogate Recoveries(%) <br /> %SSI: 106 %SS2; 99 <br /> %SS3: 97 <br /> Comments: bt <br /> water and vapor samples are reported inµg/1.,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP extracts are <br /> reported in mg/L,wipe samples inµg(wipe. <br /> ND means not detected above the reporting limit/method detection limit; N/A means analyte not applicable to this analysis; %SS=Percent Recovery of Surrogate <br /> Standard; DF=Dilution Factor <br /> Al surrogate diluted out of range or coelutes with another peak;&)low surrogate due to matrix interference. <br /> b1 aqueous sample that contains greater than-1 vol.%sediment <br /> DHS EIRP Certification 1644 - Angela Rydelius,Lab Manager <br /> Page 6 of 12 <br />