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04/09/2012 04:08 #6212 P.013/016 <br /> 1534 Willow Pass Road,Pittsburg,CA 9456 -1701 <br /> JutcCampbell Analytical, InC• httpl//Fwww.mccaTelepmpbeUsc m77)•/E-mab?maingamcca pb ll?co9m <br /> "When Quality Counts" <br /> QC SUMMARY REPORT FOR SM5520S/F <br /> W-O.Sample Matrix: Water <br /> ac Matrix: Water BatchlD:65667 WorkOrder: 1203319 <br /> EPA Method: SM552OB/F Extraction: SM552OB/F <br /> Spiked Sample.JD: NIA <br /> Sample Spiked MS MSD MS MSD L Acceptance Criteria(%) <br /> Analyte <br /> mg/L mg/L % Rec. %Rec. %RPD °h Rec. MS/MSD RPD LCS <br /> TOG N/A 20.53 N/A N/A I NIA 1 46.4 N/A NIA 70-130 <br /> Al!target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> RATQH 656(37 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID <br /> Date Sampled Date Extracted Date Analyzed <br /> 1203319-001A <br /> 03/10/12 03/12/12 03/13/12 3:30 PM J <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=laboratoryControl Sample Duplicate:7th."s' <br /> eive Percent Deviation. <br /> Recovery=100*(MS-Sample)/(Amount Spiked);RPD=100*(MS- MSD)/((MS+MSD)/2). <br /> MS J MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasample is inhomogenous AND contains <br /> significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=anal a concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sam le diluted due th matrix or anal a content. <br /> ov QA/QC Officer <br /> DHS ELAP Certification 1644 <br /> Page 9 of 12 <br />