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110 Second Avenue South,#D7,Pacheco,CA 94553 <br /> WCAWBELL ANALYTICAL INC. Telephone:510-799-1620 Fax:510-798-1622 <br /> B-mail:maiu@mccampbell.com <br /> Advanced GeoEnvironlawmtal Client Project ID:Hickinbothan Date Sampled:07/07/97 <br /> Brothers Union Safe <br /> 1803 West March Lane,Ste A Date Received:07/09/97 <br /> Stockton,CA 95207 Client Contact:Bill Little Date Extracted:07/09/97 <br /> Client P.O: Date Analyzed:07/09/97 <br /> Diesel Range(CIO-C23)Extractable Hydrocarbons as Diesel <br /> EPA methods modiW 8015,and 3550 or 3510;California RWQCB(SF Bay Region)method GCFID(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(dY %Recovery <br /> Surrogate <br /> 78400 PB3-20 S ND 101 <br /> 78401 PB3-25 S ND 101 <br /> 78405 PBI-15 S ND lot <br /> Reporting Limit unless otherwise W 50 ug/L <br /> stated;ND rneans not detected above <br /> the reporting limit S I.0 mg/kg <br /> wager and vapor samples we reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP I STLC I SPLP <br /> extracts in ug/L <br /> cluttered chromatogram resulting in eo4ated surrogate and sample peaks,or;surrogate peak is on elevated baseline,or;surrogate has been <br /> diminished by dilution of original extract <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation:a)unmodified or weakly modified diesel is significant;b)diesel range compounds are significant;no recognizable pattem;c) <br /> aged diesel?is significant);d)gasoline range compounds are significant;e)medium boiling point pattern that does not match diesel(?);f) <br /> one to a few isolated peaks present;g)oil range compounds are significant; h) lighter than water immiscible sheen is present; i)liquid <br /> sande that contains greater than--5 vol.%sediment. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />