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�i <br /> � I} <br /> Air,Water&Hazardous Waste Sampling,An ysis&Consultation <br /> COAST - TO Certified Hazardous Waste,Chemistry,Bacteriology&Bioassay Laboratories <br /> COAST' <br /> San Luis Obispo,CA•Benicia,CA +Camarillo,CA•Goleta,CA <br /> 4 ` Anaheim,CA•Tempe,AZ •Valparaiso,IN • Westbrook,ME- Indianapolis,IN <br /> Benicia Division �+ (707) 747-2757 <br /> 6006 Egret Court, Benicia, California 94510 FAX (707)747-2765 <br />, QC Batch ID: BDJ20I1 <br /> CLIENT: Coast-to-Coast Analytical Services, Inc. <br /> Analyzed 10/20/92 <br /> An, alyzed by: AZ <br /> Method'4 AS-:Listed <br /> QC SPIKE <br /> REPORT OF ANALYTICAL RESULTS Page 1 of 1 <br /> SAMPLE DESCRIPTION MATRIX SAMPLED BY SAMPLED DATE RECEIVED <br /> QC SPIKE Solid 1 <br /> 3 � <br /> CONSTITUENT *PQL SPIKE RESULT %REC NOTE <br /> mg/Kg AMOUNT mg/K9 <br /> FUEL FINGERPRINT ANALYSIS 1,2 <br /> Benzene 0.005 0.15 0.15 100. <br /> Toluene 0.01 0.36 0.34 94. <br /> Ethylbenzene 0.005 0.19 0.16 84. <br /> Xylenes, Total 0.005 0.94 0.85 90. <br /> 1,2-Dichloroethane (EDC) 0.005 NS <br /> 1,2-Dibrm-cethane (EDB) 0.005 NS <br /> Total Petroleum Hydrocarbons (Gasoline) 0.5 7.1 5.9 83. <br /> Total Petroleum Hydrocarbons (Diesel 2) 0.5 NS <br /> BTX as a percent of fuel 20. 23. <br /> 1,2-Dichioroethane-d4 (Surrogate) 0.040 0.040 100. <br /> p-Bramfluorobenzene (Surrogate) i` 0.040 0.037 93. <br /> i <br /> Benicia Division Lab Certifications: CAELAP #1719; L.A.Co-CSD#10185 <br /> * RESULTS listed as 'NS' were not spiked. PQL = Practical :�Quantitation Limit <br /> (1) ANALYZED by CAL DHS DRAFT TPH (modified) and EPA 8260 (GC/MS) <br /> (2) EXTRACTED by EPA 5030 (purge-and-trap) i{ <br /> i, <br /> �a <br /> i, <br /> i� <br /> i{IF <br /> H <br /> .i <br /> 10/27/92 Respectfully'submitted, <br /> INODS 50-387 COAST- ITO-OQAST ANALYTICAL SERVICES, INC. <br /> MH/trk/htc �� •, <br /> BD0663-3 <br /> LJ Mary Havlice ., Ph.D. <br /> President <br /> i� <br /> IF <br /> i <br />