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Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3 <br /> Job Number: C31148 <br /> Account: ENCOCALA Encon Solutions, Inc. <br /> Project: 1145 S. Aurora Street-Stockton, CA <br /> Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch <br /> C31157-9MS L29117.1) 1 12/03/13 XB n/a n/a VL919 <br /> C31157-9MSD 1-29118.13 1 12/03/13 XB n/a n/a VL919 <br /> C31157-9 a L29116.13 1 12/03/13 XB n/a n/a VL919 <br /> The QC reported here applies to the following samples: Method: SW846 8260B <br /> C31148-2, C31148-4, C31148-6, C31148-8, C31148-10, C31148-12, C31148-14, C31148-16 <br /> C31157-9 Spike MS MS MSD MSD Limits <br /> CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD <br /> 591-78-6 2-Hexanone ND 5520 5020 91 5310 96 6 68-139/24 <br /> 87-68-3 Hexachlorobutadiene ND 1380 1180 86 1200 87 2 81-126/32 <br /> 98-82-8 Isopropylbenzene ND 1380 1160 84 1210 88 4 81-122/22 <br /> 99-87-6 p-Isopropyltoluene ND 1380 1100 80*b 1120 81 2 81-121/23 <br /> 108-10-1 4-Methyl-2-pentanone ND 5520 5820 105 6150 111 6 74-136/23 <br /> 74-83-9 Methyl bromide ND 1380 1430 104 1540 112 7 82-124/20 <br /> 74-87-3 Methyl chloride ND 1380 1230 89 1380 100 11 60-132/26 <br /> 74-95-3 Methylene bromide ND 1380 1450 105 1520 110 5 82-120/20 <br /> 75-09-2 Methylene chloride ND 1380 1450 105 1520 110 5 75-119/20 <br /> 78-93-3 Methyl ethyl ketone ND 5520 6040 109 6410 116 6 71-130/22 <br /> 1634-04-4 Methyl Tert Butyl Ether ND 1380 1490 108 1560 113 5 79-127/19 <br /> 91-20-3 Naphthalene ND 1380 1230 89 1280 93 4 78-125/23 <br /> 103-65-1 n-Propylbenzene ND 1380 1080 78*b 1090 79 1 79-124/22 <br /> 100-42-5 Styrene ND 1380 1300 94 1370 99 5 83-122/21 <br /> 994-05-8 Tert-Amyl Methyl Ether ND 1380 1530 111 1620 117 6 80-127/20 <br /> 75-65-0 Tert Butyl Alcohol ND 6900 6320 92 6770 98 7 65-144/23 <br /> 630-20-6 1,1,1,2-Tetrachloroethane ND 1380 1290 94 1360 99 5 82-123/21 <br /> 71-55-6 1,1,1-Trichloroethane ND 1380 1370 99 1430 104 4 79-129/21 <br /> 79-34-5 1,1,2,2-Tetrachloroethane ND 1380 1210 88 1260 91 4 77-126/20 <br /> 79-00-5 1,1,2-Trichloroethane ND 1380 1280 93 1350 98 5 79-123/20 <br /> 87-61-6 1,2,3-Trichlorobenzene ND 1380 1210 88 1240 90 2 81-122/26 <br /> 96-18-4 1,2,3-Trichloropropane ND 1380 1240 90 1300 94 5 79-122/24 <br /> 120-82-1 1,2,4-Trichlorobenzene ND 1380 1160 84 1170 85 1 81-121/26 <br /> 95-63-6 1,2,4-Trimethylbenzene ND 1380 1220 88 1240 90 2 82-121/24 <br /> 108-67-8 1,3,5-Trimethylbenzene ND 1380 1240 90 1270 92 2 81-123/23 <br /> 127-18-4 Tetrachloroethylene ND 1380 1320 96 1360 99 3 80-125/25 <br /> 108-88-3 Toluene 42.2 J 1380 1310 92 1360 96 4 80-117/21 <br /> 79-01-6 Trichloroethylene ND 1380 1390 101 1450 105 4 81-122/20 <br /> 75-69-4 Trichlorofluoromethane ND 1380 1280 93 1390 101 8 77-133/22 <br /> 75-01-4 Vinyl chloride ND 1380 919 67*b 1020 74 10 71-133/23 <br /> 1330-20-7 Xylene(total) ND 4140 3650 88 3790 92 4 81-122/22 <br /> CAS No. Surrogate Recoveries MS MSD C31157-9 Limits <br /> 1868-53-7 Dibromofluoromethane 96% 93% 70-130% <br /> * = Outside of Control Limits. <br /> No 58 of 80 <br /> 8.a.r-.C::tJTF=S;T <br /> C31148 `...--I- <br />