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' ASSOCIATED LABORATORIES <br /> QA REPORT FORM- ORGANICS <br /> 16 Sample LR 35861 - 564 <br /> 1atnx WATER <br /> Prep Date + 04/08/99 <br /> trialysis Date 04/08/99 <br /> fWs in Batch LR 35842,35852,35861 <br /> UTRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br /> Reporting Units= mg/L <br /> Sample Spike Matrix Matrix %Ree %Rec <br /> Test Method 1 Result ND Added Spike Spike Dup MS MSD RPD <br /> TPH 8015M-G 50 U 200 242 239 121 0 119 5 1 <br /> %REC LIMITS = 70 - 130 <br />`VD— "U"-Not Detected RPD LIMITS = 30 <br /> RPD=Relative Percent Difference of Matrix Spike and Matrix Spike Duplicate <br /> 16 CMS&MSD=Percent Recovery ofMatnx Spike&Matrix Spike Duplicate <br /> REPARATION BLANK/LAB CONTROL SAMPLE RESULTS <br />' PREP BLANK LCS <br /> Value ND Result True %Rec L Limit ILLmut <br /> 50 U 309 300 1030 80% 120% <br /> Value=Preparation Blank Value ND= "U"for Not-Detected <br /> t <br /> CS Result=Lab Control Sample Result <br /> rue=True Value of LCS <br /> L.Limit/HLimit=LCS Control Limits <br /> 4/22/99 8015m-g_tPh_0408W AS <br />