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ASSOCIATED LABORATORIES <br /> QA REPORT FORM <br /> QC Sample LR 69549-610 <br /> Matrix WATER <br /> Prep Date 03/25/01 <br /> Analysis Date _03/25/01-03/26/01 <br /> ID#'s in Batch LR 69549,69848 <br /> MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br /> Reporting Units=ug/L <br /> Sample Spike Matrix Matrix %Rec %Rec <br /> Test Method Result Added Spike SpikeDup MS MSD RPD <br /> TPH 80t5M-G ND 200 185 186 925 930 05 <br /> ND=Not Detected <br /> RPD=Relame Percent Difference of Matrix Spike and Matrix Spike Duplicate %REC LIMITS = 70 - 130 <br /> lie <br /> %REC-MS&AISD=Percent Recovery of Matrix Spike&Matrix Spike Duplicate jPPQLlVf1TS = 30 <br /> PREPARATION BLANK/LAB CONTROL SAMPLE RESULTS <br /> PREP BLK LCS <br /> Value Result True %Ree L.Limit H Limit <br /> ND 174 200 870 80% 120% <br /> LCS Result=Lab Control Sample Result <br /> True=True Value of LCS <br /> L Limit/H Limit=LCS Control Limits <br /> 04/43/2001 8015g_tph_0325w x!s <br />