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0 <br />(D.Sequoia <br />iqW Analytical <br />0 <br />819 Striker Ave Ste 8 <br />Sacramento, CA 95834 <br />{9 16) 921.9600 <br />FAX (9 16) 92 1 -0 100 <br />www.sequaialabs.com <br />Kleinfelder - Stockton Project: SJCM & VCD 5310384 <br />2825 East Myrtle Street Project Number: 36274 Reported: <br />Stockton CA, 95205 Project Manager: Doug Heard 11/05/03 14:50 <br />Organochlorine Pesticides by EPA Method 8081A <br />Star Analytical, Inc. <br />Reporting <br />Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes <br />26653,-54,-55,-56 (Composite) (5310384-02) Solt <br />Sampled: 10/14/03 14:06 Received: 10/16/03 08:49 <br />Heptachlor <br />ND <br />2.00 <br />ug/kg I V3J2905 10/28/03 11/04/03 EPA 8081A <br />Heptachlor epoxide <br />ND <br />2,00 <br />" <br />Methoxychlor <br />ND <br />20.0 <br />" <br />Toxaphene <br />ND <br />80.0 <br />" <br />Surrogate: TCMX <br />67.1 % <br />29.1-172 " <br />Surrogate: Decachloroblphenyl <br />70.1 % <br />12.9-225 " <br />26657,-58,-59,-60 (Composite) (5310384-03) Soil <br />Sampled: 10/14/03 <br />15:05 Received: 10/16/03 08:49 A-02 <br />Aldrin <br />ND <br />10.0 <br />ug/kg 10 V3J2805 10/28/03 11/05/03 EPA 8081 A <br />alpha -BHC <br />ND <br />10.0 <br />" <br />beta -BHC <br />ND <br />10.0 <br />" <br />delta -BHC <br />ND <br />10.0 <br />" <br />gamma -BHC (Lindane) <br />ND <br />10.0 <br />" <br />alpha -Chlordane <br />ND <br />50.0 <br />" <br />gamma -Chlordane <br />ND <br />20.0 <br />" <br />4,4' -DDD <br />ND <br />60.0 <br />4,4' -DDE <br />ND <br />60.0 <br />" <br />4,4' -DDT <br />ND <br />60.0 <br />Dieldrin <br />ND <br />20.0 <br />" <br />Endosulfan I <br />ND <br />20.0 <br />Endosulfan II <br />ND <br />20.0 <br />" <br />Endosulfan sulfate <br />ND <br />60.0 <br />" <br />Endrin <br />ND <br />20.0 <br />" <br />Endrin aldehyde <br />ND <br />60.0 <br />" <br />Heptachlor <br />ND <br />20.0 <br />" <br />Heptachlor epoxide <br />ND <br />20.0 <br />" <br />Methoxychlor <br />ND <br />200 <br />Toxaphene <br />ND <br />800 <br />" <br />Surrogate: TCMX <br />130 % <br />29.1-172 " <br />Surrogate: Decachlorobiphenyl <br />% <br />12.9-225 5-06 <br />Sequoia Analytical - Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br />custody document. Unless otherwise stated, results are reported on a wet weight basis. <br />This analytical report must be reproduced in its entirety. <br />Page 24 of 44 <br />