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Alpha Analytical, Inc. <br />Ak, 255GlendaleAve. • Suite 21 • Sparks, Nevada 8943778 <br />(775) 355-1044 - (775) 355-0406 FAX • 1-800-283-1183 <br />Kleinfelder <br />2825 East Myrtle Street <br />Stockton, CA 95205 <br />Job#: 36274/SJCM+VCD <br />Alpha Analytical Number: KLF03110343-04A <br />Client I.D. Number: 26699-MW4 <br />ANALYTICAL REPORT <br />Attn: Doug Heard <br />Phone: (209) 948-1345 <br />Fax: (209)948-0621 <br />Volatile Organics by GC/MS <br />EPA Method SW8260B <br />Some Reporting Limits were increased due to high concentrations of target analytes. <br />Sampled: 10/29/03 <br />Received: 11/01/03 <br />Analyzed: 11/05/03 <br />Reporting <br />Compound Concentration Limit <br />Compound <br />Concentration <br />Reporting <br />Limit <br />1 <br />Chloromethane <br />NO <br />4.0 pg/L <br />2 <br />Vinyl chloride <br />ND <br />1.0 pg/L <br />3 <br />Chloroethane <br />NO <br />1.0 pg/L <br />4 <br />Bromomethane <br />NO <br />1.0 pg/L <br />5 <br />Trichlorofluoromethane <br />NO <br />1.0 pg/L <br />6 <br />1,1-Dichiorcethene <br />NO <br />1.0 pg/L <br />7 <br />Tertiary Butyl Alcohol (TBA) <br />150 <br />10 pg/L <br />6 <br />Dichloromethane <br />ND <br />4.0 pg/L <br />9 <br />trans-1,2-DicNoroethene <br />NO <br />1.0 pglL <br />10 <br />Methyl tert-butyl ether (MTBE) <br />790 <br />0.50 pg/L <br />11 <br />1,1-Dichloroethane <br />NO <br />1.0 pg/L <br />12 <br />01-isopropyi Ether (OIPE) <br />NO <br />1.0 pg/L <br />13 <br />cis- 1,2-Dichloroethene <br />NO <br />1.0 pg/L <br />14 <br />Chloroform <br />NO <br />1.0 pg/L <br />15 <br />Ethyl Tertiary Butyl Ether (ETRE) <br />NO <br />1.0 pg/L <br />16 <br />1,2-Dichloroethane <br />NO <br />1.0 pg/L <br />17 <br />1,1,1 -Trichloroethane <br />NO <br />1.0 pg/L <br />18 <br />Carbon tetrachloride <br />NO <br />1.0 P911- <br />glL19 <br />19 <br />Benzene <br />NO <br />0.50 pg/L <br />20 <br />Tertiary Amyl Methyl Ether (TAME) <br />1.5 <br />1.0 pg/L <br />21 <br />1,2-Dichloropropane <br />NO <br />1.0 pg/L <br />22 <br />Trichloroethene <br />NO <br />1.0 Pg/1- <br />glL23 <br />23 <br />Bromodichloramethane <br />ND <br />1.0 pg/L <br />24 <br />cis-1,3-Dichicropropene <br />NO <br />1.0 pg/L <br />25 <br />trans-1,3-Dichloroprcpene <br />NO <br />1.0 pg/L <br />Some Reporting Limits were increased due to high concentrations of target analytes. <br />Sampled: 10/29/03 <br />Received: 11/01/03 <br />Analyzed: 11/05/03 <br />Reporting <br />Compound Concentration Limit <br />26 1,1,2 -Trichloroethane <br />Na <br />1.D pg/L <br />27 Toluene <br />NO <br />0.50 pg/L <br />28 Dibromochloromethane <br />NO <br />1.0 pg/L <br />29 Tetrachloroethene <br />NO <br />1,0 pg/L <br />30 Chlorabenzene <br />NO <br />1,0 pg/L <br />31 Ethylbenzene <br />NO <br />0.50 pglL <br />32 m,p-Xylene <br />NO <br />0.50 pg/L <br />33 Bromoform <br />NO <br />1.0 pg/L <br />34 a-Xyiene <br />NO <br />0.50 pg/L <br />35 1.1,2,2•Tetrachiaroethane <br />NO <br />1.0 pg/L <br />36 1,3 -Dichlorobenzene <br />NO <br />1.0 pg/L <br />37 1,4 -Dichlorobenzene <br />NO <br />1.0 pg/L <br />36 1,2 -Dichlorobenzene <br />ND <br />1.0 pg/L <br />ND = Not Detected <br />Roger L. Scholl, Ph.D., Laboratory Director • • Randy Gardner, laboratory Manager • • Walter Hinchman, Quality Assurance Officer <br />Sacramento, CA • (916) 366-9089 / Las Vegas, NV • (702) 281-4848 / Wichita, KS • (316) 722-58901 info®alpha-analyticalcom <br />1117103 <br />Report hate <br />