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GeoAnalytical Laboratories; Irig fel ,� � -� <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax (209)� PQM a-Ai- NE* { <br /> f� <br /> IT aERVIC <br /> .03 MA Y l 3 Q <br /> CERTIFICATE OF ANALYSIS � <br /> Report# P122-12 Oxygenates �f Date: 51 <br /> y 1 <br /> Thorpe Oil Protect: Thorpe's Yard Date Rec'd: 5/02! Date Started: 5/06/,03 <br /> PO Box 357 E, Date Completed:5/06% k <br /> Lodi CA 95241 PO# �� k <br />! I <br /> Dake Sampled: 5/02/03 4 <br /> I} Sampler: R.Azevedo(Geo) <br /> Sample ID Lab ID RL Method Analyte Results Units <br /> Line le#1 @ 4 <br /> Sam ' <br /> P200646 10 8260B Methyl tert-butyl ether{MTBE) ND µg/Kg <br /> Sample 400 Ethanol 1) ND <br /> 200 tert-ButanolL NU <br /> 10 di-Isopropyl ether(DiIPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND i <br /> I <br /> Surrogate Amnt Spiked Amnt Rec.. %Recovery QC it% <br /> 1,2-Dichloroethane-d4 2Lim <br /> 0 20.3 101.5 66-133 <br /> 2-Bromo-l-chloropropane 20 22.5 112.5 63-139 <br /> 4-Bromofluorobenzene 20 18.5 92.5 64-136 i <br /> I�I ND /K <br /> 4' P200647 10 826QB Methyl tert-butyl ether(MTBE) Ag/Kg <br /> Line Sample#2® <br /> 400 Ethanal ND <br /> 200 tent-Butanol f ND <br /> 10 di-Isopropyl ether(RIPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND i <br /> 10 tent-Amyl methyl ether(TAME) ND <br /> (J n <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% ) <br /> 1,2-Didloroethme-d4 F¢20 20.6 103.0 66-133 <br /> 2-Bromo-1-chloropropane �,20 1 23.6 118.0 63-139 <br /> ` 4-Bromofluorobenzene li20 17.2 86.0 64-136 <br /> 1' <br /> Line Sample#3®4' P200648 10 8260B Methyl tert-butyl ether(MTBE) ND µg/Kg 1 <br /> 400 Ethanol I; ND <br /> 200 tent-Butanol; ND <br /> 10 di-Isopropyll ether{DIPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND F <br /> 10 tent-Amyl methyl ether(TAME) ND <br /> I} <br /> Surrogate Amnt Spiked:1 <br /> Amort Rec. %Recovery QC Limit% <br /> s 1,2-Dichloroethane-d4 hI 20 25.7 128.5 66-133 <br /> 2-Bromo-l-&doropropane 11120 24.3 121.5 63-139 <br /> 4-Bromofluorobenzene JJ 20 18.3 91.5 64-136 <br /> L C � <br /> Mario D'Onofrio Donna.Keller <br /> ' Certification # 115T Laboratory Director <br /> Chemist <br />